Agarwood leaf-based wood flavor flavor for tobacco and its preparation method and application
A kind of technology of agarwood leaf and woody fragrance, applied in essential oils/spices, application, tobacco, etc., can solve the problems of low overall utilization rate of white woody fragrance resources and difficulty in obtaining economic benefits, achieve good economic and social benefits, increase alcohol and Degree, improve the effect of absorbing flavor
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Embodiment 1
[0023] Grind the leaves of A. chinensis through a 40-mesh sieve, add distilled water 4 times the weight of the powder of A. chinensis and 0.7% of a compound enzyme relative to the weight of the powder of A. chinensis, that is, β-glucanase 3.5 million U / mL, Cellulase 150,000 U / mL, hemicellulase 1.5 million U / mL, pectinase 10,000 U / mL, the volume ratio of the four enzymes is 1:3:2:1,
[0024] 40 ℃ water bath constant temperature treatment for 3h. Add ethanol until the total solvent is 8 times the mass of Akiras sinensis leaf powder, heat reflux at 70°C for 1.5h, and extract 3 times, combine the extracts and then concentrate under reduced pressure to the state of extract, place the extract in supercritical CO 2 In the extraction kettle, add 100% ethanol with a concentration of 0.7 times of the weight of the raw material of Akira sinensis leaf powder, set the extraction pressure of the extraction kettle to 22MPa, the extraction temperature to 45°C, the extraction time to 3h, CO 2...
Embodiment 2
[0028] Grind the leaves of A. chinensis through a 60-mesh sieve, add distilled water 6 times the weight of the powder of A. chinensis and 0.3% of a compound enzyme relative to the weight of the powder of A. chinensis, that is, β-glucanase 3.5 million U / mL, Cellulase 150,000 U / mL, hemicellulase 1.5 million U / mL, pectinase 10,000 U / mL, the volume ratio of the four enzymes is 1:2:2:1,
[0029] 60 ℃ water bath constant temperature treatment for 1h. Add ethanol until the total solvent is 10 times the mass of Akiras sinensis leaf powder, heat reflux at 90°C for 0.5h, and the extraction frequency is 1 time, combine the extracts and then concentrate under reduced pressure to the state of extract, and place the extract in supercritical CO 2 In the extraction kettle, add 90% ethanol with a concentration of 0.3 times the weight of the raw material of the white wood root powder, set the extraction pressure of the extraction kettle to 28MPa, the extraction temperature to 50°C, the extracti...
Embodiment 3
[0033]Grind the leaves of A. chinensis through a 50-mesh sieve, add distilled water 5 times the weight of the powder of A. chinensis and 0.5% of a compound enzyme relative to the weight of the powder of A. chinensis, that is, β-glucanase 3.5 million U / mL, Cellulase 150,000 U / mL, hemicellulase 1.5 million U / mL, pectinase 10,000 U / mL, the volume ratio of the four enzymes is 1:2:2:2,
[0034] 50 ℃ water bath constant temperature treatment for 2h. Add ethanol until the total solvent is 9 times the mass of Akiras sinensis leaf powder, heat reflux extraction at 80°C for 1 hour, and extract twice, combine the extracts and then concentrate under reduced pressure to the state of extract, place the extract in supercritical CO 2 In the extraction kettle, add 95% ethanol with a concentration of 0.5 times the weight of the raw material of the white wood root powder, set the extraction pressure of the extraction kettle to 25MPa, the extraction temperature to 47°C, the extraction time to 2.5...
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