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A kind of preparation method of Maillard reaction product particles of tobacco leaf extract

A technology of Maillard reaction and tobacco leaf extract, which is applied in the field of preparation of Maillard reaction product granules, can solve the problems of unobvious characteristic aroma and insufficient aroma, achieve good market prospects and application value, easy to obtain, and high uniformity The effect of sex and intensity

Active Publication Date: 2018-03-20
CHINA TOBACCO GUANGXI IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Smoking and health have become a common concern all over the world. One of the ways to deal with this problem in my country's tobacco industry is to reduce harm and reduce coke. However, while reducing harm and coke, it is inevitable that there will be problems of insufficient aroma and unobvious characteristic aroma.

Method used

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  • A kind of preparation method of Maillard reaction product particles of tobacco leaf extract
  • A kind of preparation method of Maillard reaction product particles of tobacco leaf extract
  • A kind of preparation method of Maillard reaction product particles of tobacco leaf extract

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Firstly take the tobacco leaves and chop them up, use 20 times of water as the solvent to heat and extract at 100°C, and then obtain the tobacco leaf extract through hot filtration and refrigerated sedimentation filtration, and the concentrated yield is 23.95% of the tobacco leaf extract; Take 5g of tobacco paste mixture with an acid content of 10:1, weigh 100g of a mixed solvent with a mass ratio of triacetin:glycerol of 10:1, put the tobacco paste mixture into the mixed solvent, and heat it at 100°C for 12 hours to obtain tobacco leaves The Maillard reaction product of the extract; the Maillard reaction product of the triacetin layer is a yellow or brownish-yellow transparent liquid, weigh 1g, stir with the excipient material mass ratio of 120:1, weigh 0.1g lemon Dissolve sodium bicarbonate and 9.9g glucose in 95mL water, magnetically stir to dissolve completely, then spray it evenly into 110g corn porous starch and mix well to form a moist composite powder, and pass t...

Embodiment 2

[0028] Firstly take the tobacco leaves and chop them up, use 15 times of ethanol as a solvent to heat and extract at 100°C, and obtain the tobacco leaf extract through hot filtration and refrigerated sedimentation filtration, and the concentrated yield is 23.70% of the tobacco leaf extract; Take 5g of the tobacco cream mixture with a ratio of 9:1, weigh 100g of a mixed solvent with a mass ratio of glycerol triacetate:glycerol of 8:1, put the smoke cream mixture into the mixed solvent, and heat it at 100°C for 10 hours to obtain tobacco leaves The Maillard reaction product of the extract; the Maillard reaction product of the triacetin layer is a yellow or brownish yellow transparent liquid, weigh 1g, stir with the excipient material at 150:1, weigh 0.1g sodium citrate and 9.9g of glucose were dissolved in 100mL of water, magnetically stirred to dissolve completely, and then evenly sprayed into 140g of glutinous rice flour and mixed well to form a moist composite powder, which wa...

Embodiment 3

[0029] Example 3 Tobacco leaves were firstly taken and chopped, heated and extracted with 10 times of ethanol as a solvent at 60°C, filtered through hot filtration and refrigerated sedimentation to obtain tobacco leaf extract, and the concentration yield was 23.20% of tobacco leaf extract; then the tobacco extract was weighed: Take 5g of smoke paste mixture with a mass ratio of proline of 2:1, weigh 100g of a mixed solvent with triacetin:glycerol with a mass ratio of 0.5:1, put the smoke paste mixture into the mixed solvent, and heat it at 100°C for 3 hours, the Maillard reaction product of the tobacco leaf extract was obtained; the Maillard reaction product of the triacetin layer was a yellow or brownish-yellow transparent liquid, weighed 0.5g, stirred at 100:0.5 with the excipient material, weighed Dissolve 0.1g of sodium malate and 6.9g of sucrose in 90mL of water, magnetically stir to dissolve completely, then evenly spray it into 93g of corn porous starch and mix well to f...

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PUM

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Abstract

The invention discloses a preparation method of Maillard reactant particles of tobacco leaf extract. Tobacco leaves are firstly taken and chopped, heated and extracted with water or ethanol as a solvent, the tobacco leaf extract is obtained by hot filtration and refrigerated sedimentation filtration, and concentrated to obtain tobacco leaf extract; then the mixture of tobacco extract and amino acids is added to glycerol triacetate and mixed In the solvent, the heating time at 80-100°C is 3-12 hours to obtain the Maillard reaction product of the tobacco leaf extract; the Maillard reaction product of the triacetin layer is a yellow or brownish-yellow transparent liquid, the same as the excipient material Stir and mix to form wet composite powder, and obtain Maillard reaction product granules of tobacco leaf extract through granulation, microwave setting, microwave drying, granule cooling and sieving. The Maillard reactant of granular tobacco leaf extract prepared by the invention is applied to cigarette filter sticks, which can effectively compensate for the decline in cigarette aroma caused by filter stick filtration and perforation dilution, and improve the smoking quality of cigarettes.

Description

technical field [0001] The invention relates to the field of cigarette material preparation, in particular to a method for preparing maillard reaction product granules of tobacco leaf extract. Background technique [0002] Smoking and health have become a common concern all over the world. One of the ways to deal with this problem in my country's tobacco industry is to reduce harm and reduce coke. However, while reducing harm and coke, it is inevitable that there will be problems of insufficient aroma and unobvious characteristic aroma. . As a bridge between the smoker and the mainstream smoke, the mouth stick can not only filter some harmful components in the smoke and reduce the tar content, but also can effectively compensate for the natural smoke aroma of cigarettes through reasonable mouth stick flavoring technology. [0003] Tobacco leaf extract (tobacco paste) is a paste that is extracted and concentrated from tobacco leaf raw materials by ethanol or water. It can enh...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B9/00A24D3/14
Inventor 王萍娟李志华张雨夏田玉红冯守爱黄东业吴彦田兆福周俊宋凌勇李小兰
Owner CHINA TOBACCO GUANGXI IND
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