Coating composition
A composition and coating technology, applied in polyester coatings, coatings, layered products, etc., can solve the problems of affecting the storage stability of the composition, reducing the antifouling performance, and the coating film being insufficient to maintain the antifouling performance, etc. Effects of good storage stability, retention of antifouling properties, good film hardness and processability
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[0087] The polymerization initiator used in the preparation of the copolymer resin (d) is a polymerization initiator or the like commonly used in a method for producing an acrylic polymer. The amount of the polymerization initiator is usually 0.1% by mass to 20% by mass based on the total amount of the polymerizable unsaturated monomer (d1) and another polymerizable unsaturated monomer (d2).
[0088] Examples of the polymerization initiator include azo polymerization initiators such as 2,2'-azobisisobutyronitrile, azobis-2-methylbutyronitrile, and azobisdivaleronitrile; t-butyl peroxyisobutyrate ester, tert-butyl peroxy-2-ethylhexanoate, tert-amyl peroxy-3,5,5-trimethylhexanoate, tert-butyl peroxyisopropyl carbonate, 2,2-bis(4 , 4-di-tert-butylperoxycyclohexyl) propane and organic peroxide polymerization initiators.
[0089] Any known method can be used as a method for obtaining the copolymer resin (d). Among them, the solution polymerization method is preferable. An exampl...
Embodiment
[0123] The present invention is described in more detail below with reference to Examples and Comparative Examples. The present invention is not limited by the following examples. "Parts" and "%" as shown below are based on mass.
[0124] Preparation of hydroxyl-containing polyester resin (a)
preparation example 1-
[0125] Preparation Example 1-Preparation of Polyester Resin Solution (Component a1)
[0126] 1079 parts of isophthalic acid, 407 parts of adipic acid, 466 parts of neopentyl glycol and 802 parts of trimethylolpropane were placed in a reaction device equipped with a thermometer, stirrer, heater and distillation column, and heated to 160 ℃. The temperature was further increased gradually from 160°C to 230°C over 3 hours.
[0127] Then, after allowing the reaction to proceed at 230° C. for 30 minutes, the distillation column was replaced by a water separator. 124 parts of xylene were added to the mixture, and xylene was also added to the water separator to azeotrope the water and xylene, and remove condensed water. The resulting mixture was reacted until an acid value of 10 mg KOH / g was reached. After cooling the mixture, 855 parts of cyclohexanone was added to provide a polyester resin solution having a solid content of 55%. The obtained resin had a hydroxyl value of 184 mg ...
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