curable composition
A composition and average composition technology, applied in the field of curable compositions, can solve the problems of encapsulants not having heat resistance and light resistance
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Embodiment 1
[0161] Surface treatment of inorganic fillers
[0162] 20 g of an aqueous dispersion of silicon dioxide (solid content: 40% by weight, average diameter of silicon dioxide: 10 nm) was diluted with 70 g of ethanol, and then mixed with a surface treatment solution (by dissolving 15 g of both ends in 50 g of isopropanol) Hydroxyl methylphenyl oligomers (prepared by aryl molar ratio (Ar / Si): 0.4)) were mixed, and the resulting mixture was kept at room temperature for 3 days. Thereafter, unreacted substances were washed and distilled under reduced pressure to obtain a surface-treated inorganic filler.
[0163] Preparation of Curable Compositions
[0164] The curable composition is prepared by mixing compounds prepared by a known method and represented by formulas A to D so as to be curable by hydrosilylation reaction (mixing amount: compound of formula A: 80 g, compound of formula B: 20 g, Compound of formula C: 200 g, compound of formula D: 70 g). Subsequently, a catalyst (pla...
Embodiment 2
[0174] 20 g of an aqueous dispersion of silicon dioxide (solid content: 40% by weight, average diameter of silicon dioxide: 10 nm) was diluted with 70 g of ethanol, and then mixed with a surface treatment solution (by dissolving 15 g of both ends in 50 g of isopropanol) Hydroxyl methylphenyl oligomers (prepared by aryl molar ratio (Ar / Si): 0.9)) were mixed, and the resulting mixture was kept at room temperature for 3 days. Thereafter, unreacted substances were washed and distilled under reduced pressure to obtain a surface-treated inorganic filler. A curable composition was prepared as described in Example 1 except that the above-mentioned inorganic filler was used.
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