Crude oil pour-point depressant and preparation method thereof
A crude oil pour point depressant and solvent technology, applied in chemical instruments and methods, drilling compositions, etc., can solve problems such as insurmountable influence
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Embodiment 1
[0017] (1) First synthesize polystyrene maleic anhydride:
[0018] Add 4.9g of maleic anhydride and 0.1g of benzoyl peroxide (BPO) into 75ml of toluene solvent, add 5.2g of styrene after fully dissolved, raise the temperature to 50°C under the protection of nitrogen, stir for 15min to make the maleic anhydride completely Dissolve, then heat up to 80°C and react for 1 hour to obtain polystyrene maleic anhydride, a milky white paste product. The reactant is cooled to room temperature, and the product is filtered out, and dried in vacuum at 60°C;
[0019] (2) Esterification of polystyrene maleic anhydride:
[0020] Add 3.06g of polystyrene maleic anhydride and 0.2g of p-toluenesulfonic acid into 70ml of toluene, fully dissolve, add n-octanol, stir and heat, condense and reflux for 6h, and after cooling, a light yellow jelly-like substance is obtained; n-octanol and The molar ratio of maleic anhydride is 1:1;
[0021] (3) Preparation of crude oil pour point depressant: 100% by w...
Embodiment 2
[0024] (1) First synthesize polystyrene maleic anhydride:
[0025] Add 4.9g of maleic anhydride and 0.1g of benzoyl peroxide (BPO) into 75ml of toluene solvent, add 5.2g of styrene after fully dissolved, raise the temperature to 50°C under the protection of nitrogen, stir for 15min to make the maleic anhydride completely Dissolve, then raise the temperature to 80°C-85°C and react for 1 hour to obtain a milky white paste product polystyrene maleic anhydride, the reactant is cooled to room temperature, the product is filtered out, and vacuum-dried at 60°C;
[0026] (2) Esterification of polystyrene maleic anhydride:
[0027] Add 3.06g of polystyrene maleic anhydride and 0.2g of p-toluenesulfonic acid into 70ml of toluene, fully dissolve, add C20 alcohol, stir and heat, condense and reflux for 6h, and obtain a light yellow jelly substance after cooling; C20 alcohol and polyphenylene The molar ratio of ethylene maleic anhydride is 1:1;
[0028] (3) Preparation of crude oil pour ...
Embodiment 3
[0031] (1) First synthesize polystyrene maleic anhydride:
[0032] Add 4.9g of maleic anhydride and 0.1g of benzoyl peroxide (BPO) into 75ml of toluene solvent, add 5.2g of styrene after fully dissolved, raise the temperature to 50°C under the protection of nitrogen, stir for 15min to make the maleic anhydride completely Dissolve, then heat up to 85°C and react for 1 hour to obtain polystyrene maleic anhydride, a milky white paste product. The reactant is cooled to room temperature, the product is filtered out, and vacuum-dried at 60°C;
[0033] (2) Esterification of polystyrene maleic anhydride:
[0034] Add 3.06g of polystyrene maleic anhydride and 0.2g of p-toluenesulfonic acid into 70ml of toluene. After fully dissolving, add the mixture of C18 alcohol, C20 alcohol and C24 alcohol, stir and heat, condense and reflux for 6 hours. After cooling, a light yellow jelly-like substance is obtained. ; The molar ratio of C18 alcohol, C20 alcohol and C24 alcohol mixture to polystyr...
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