Anti medroxyprogesterone specific monoclonal antibody hybridoma cell strain and application thereof
A hybridoma cell line, monoclonal antibody technology, applied in biochemical equipment and methods, microorganisms, microorganism-based methods, etc., can solve problems such as difficulty in obtaining accurate and objective results, achieve good application value, simple synthesis process, High sensitivity effect
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[0029] (1) Preparation of medroxyprogesterone hapten: 34.4 mg (0.1 mmol) of medroxyprogesterone was dissolved in 3 mL of anhydrous dimethyl sulfoxide to obtain liquid A, and 27.8 mg (0.2 mmol) of dibromoacetic acid was dissolved in 1.4 mL In anhydrous dimethyl sulfoxide, obtain liquid B, add potassium hydroxide powder 208.5 mg (1.5 mmol) to liquid A, stir at room temperature until the color of the solution turns slightly yellow, add liquid B dropwise to liquid A, The yellow color gradually deepened, reacted at room temperature for 4 hours, terminated the reaction with 50 mL of ice water, extracted three times with ethyl acetate, combined the water phase, acidified the water phase with 2 mol / L hydrochloric acid to obtain a yellow precipitate, washed four times with water until neutral, and dried to obtain a yellow color Medroxyprogesterone Hapten (MP-2CME) Powder.
[0030] The product was identified by LC-MS after dissolving in methanol.
[0031] (2) Preparation of Medroxyprog...
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