A kind of preparation method of composite shell type microcapsule
A technology of microcapsules and capsule cores, which is applied in the fields of chemical engineering and new material production, and can solve problems such as difficulty in application, poor mechanical strength of microcapsules, resistance to acids and alkalis, etc.
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[0020] 1. Preparation process:
[0021] Accurately weigh a certain mass ratio of dichloromethane, sodium lauryl sulfate, Span 80 and sodium chloride (or cerium oxide, potassium permanganate) in a three-necked flask, stir and react for 10 minutes, then slowly add quantitative The butyl titanate was refluxed for 20 minutes at 70°C, and then a certain amount of polyethylene (or polypropylene, poly-n-butyl acrylate) was added to the reaction device. After continuing the reaction for a period of time, the temperature of the system was lowered to normal temperature (25°C), and a certain amount of mixed solution of n-butyl ether and epoxy resin was slowly added, and the system was stirred and reacted for 2 hours to obtain composite shell-type microcapsules.
[0022] The following specific embodiments help to understand the present invention, but do not limit the content of the present invention.
[0023] The percentage (100%) of each component accounting for the total weight of the ...
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