Multiscale reaction carrier with porous microchannel structure and its preparation method
A technology of micro-channel structure and reaction carrier, which is applied to catalyst carriers, chemical instruments and methods, physical/chemical process catalysts, etc. problems such as decline, to achieve the effect of being conducive to cascading expansion, large-scale promotion, and improving the reaction rate and conversion rate
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[0044] Such as image 3 As shown, the preparation method of the present invention adopts the surface sintering dissolution method, and the specific preparation process includes the following steps:
[0045] 1) Grinding: the aluminum alloy powder and salt powder are ball-milled into small particles, and the upper surface of the lower die punch 5 of the mold is provided with micro-grooves, and the cross-section of the micro-grooves is an inverted trapezoid;
[0046] 2) Powder spreading: Evenly drop a layer of absolute ethanol on the upper surface of the lower die punch 5, and then evenly spread a layer of salt powder particles 7, then evenly spread aluminum alloy powder particles 8 on the salt powder particle layer, and then put After punching 6, the upper die is placed in the female die 4, such as figure 2 shown;
[0047] 3) Cold pressing: cold pressing in the mold, the pressure is 100-400MPa, keep for 6-10 minutes;
[0048] 4) Hot pressing: place the mold in a resistance f...
Embodiment 1
[0061] The preparation method of the present invention adopts the surface sintering dissolution method, and the specific preparation process is:
[0062] The first step is to grind and spread powder, such as figure 2 As shown, the aluminum alloy powder and salt powder are ground into particles of suitable size, the size of the aluminum alloy powder particle 8 is about 20 μm, and the particle size of the salt powder particle 7 is about 50 μm; In the microchannel 2, a layer of absolute ethanol is evenly dripped on the upper surface, and then a layer of salt powder particles 7 is evenly spread, and then the aluminum alloy powder particles 8 are evenly spread on the top of the salt powder particles 7. The thickness of the salt powder particles 7 is about 300 μm, and the thickness of the aluminum alloy powder particles 8 is about 1.5 mm.
[0063] In the second step, cold pressing is carried out in a mold with a pressure of 100 MPa and kept for 10 minutes.
[0064] The third step...
Embodiment 2
[0087] The preparation method of the present invention adopts the surface sintering dissolution method, and the specific preparation process is:
[0088] The first step is to grind and spread powder, such as figure 2 As shown, the aluminum alloy powder and the salt powder are respectively ground into particles of suitable sizes, the size of the aluminum alloy powder particles 8 is about 50 μm, and the particle size of the salt powder particles 7 is about 180 μm; For the trapezoidal microchannel 2, a layer of absolute ethanol is evenly dripped on the upper surface, and then a layer of salt powder particles 7 is evenly spread, and then the aluminum alloy powder particles 8 are evenly spread on the top of the salt powder particles 7, and the salt powder particles 7 The thickness is about 350 μm, and the thickness of the aluminum alloy powder particles 8 is about 1.8 mm.
[0089] In the second step, cold pressing is carried out in a mold with a pressure of 300 MPa and kept for 8...
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Abstract
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