Preparation method of composite biological filler for spiral groove
A technology of spiral groove and biological filler, which is applied in the field of preparation of spiral groove composite biological filler, can solve the problems of poor dispersion, poor adsorption performance, poor stability, etc., and achieve increased mixing degree, good adsorption performance, and good dispersion. Effect
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Embodiment 1
[0021] (1) Take the coconut shell, crush it, pulverize it with a superfine pulverizer and refine it with a superfine pulverizer to obtain powder particles with a particle size of about 200 mesh, and set aside;
[0022] (2) Weigh 100 parts by mass of vermiculite, crush it with a pulverizer and sieve it to obtain vermiculite powder with a particle size of less than 200 mesh, put it in a muffle furnace, and raise the temperature to 300°C at a heating rate of 10°C / min After cooling to room temperature naturally, soak 50 parts by mass of 2-pyrrolidone-5-sodium carboxylate for 5 hours to form a solid-liquid mixture, then add dehydrated ethanol to it and stir evenly, and then drop it into the above-mentioned solid-liquid mixture at 30°C Add 5 parts by mass of silver nitrate solution with a concentration of 1 mol / L, stir while adding it dropwise, then leave it to stand for 2 hours and then centrifuge, take out the solid matter, wash it 3 times with absolute ethanol, and then place the ...
Embodiment 2
[0033] (1) Take the coconut shell, crush it, pulverize it with a superfine pulverizer and refine it with a superfine pulverizer to obtain powder particles with a particle size of about 200 mesh, and set aside;
[0034] (2) Weigh 100 parts by mass of vermiculite, crush it with a pulverizer and sieve it to obtain vermiculite powder with a particle size of less than 200 mesh, put it in a muffle furnace, and raise the temperature to 300°C at a heating rate of 10°C / min After cooling to room temperature naturally, soak 50 parts by mass of 2-pyrrolidone-5-sodium carboxylate for 5 hours to form a solid-liquid mixture, then add dehydrated ethanol to it and stir evenly, and then drop it into the above-mentioned solid-liquid mixture at 30°C Add 5 parts by mass of silver nitrate solution with a concentration of 1 mol / L, stir while adding it dropwise, then leave it to stand for 2 hours and then centrifuge, take out the solid matter, wash it with absolute ethanol for 3 to 5 times, then place...
Embodiment 3
[0045] (1) Take the coconut shell, crush it, pulverize it with a superfine pulverizer and refine it with a superfine pulverizer to obtain powder particles with a particle size of about 200 mesh, and set aside;
[0046] (2) Weigh 100 parts by mass of vermiculite, crush it with a pulverizer and sieve it to obtain vermiculite powder with a particle size of less than 200 mesh, put it in a muffle furnace, and raise the temperature to 300°C at a heating rate of 10°C / min After cooling to room temperature naturally, soak 50 parts by mass of 2-pyrrolidone-5-sodium carboxylate for 5 hours to form a solid-liquid mixture, then add dehydrated ethanol to it and stir evenly, and then drop it into the above-mentioned solid-liquid mixture at 30°C Add 5 parts by mass of silver nitrate solution with a concentration of 1 mol / L, stir while adding it dropwise, then leave it to stand for 2 hours and then centrifuge, take out the solid matter, wash it with absolute ethanol for 3 to 5 times, then place...
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