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Method for preparing microcapsule clove essential oil and application of clove essential oil in tobacco

A technology of clove essential oil and microcapsules, which is applied in the fields of essential oils/spices, tobacco, applications, etc., can solve problems such as no public literature reports, and achieve the effects of improving cigarette smoking quality, reducing irritation, and reducing cigarette miscellaneous gas

Inactive Publication Date: 2014-12-03
NANJING BIAOKE BIO TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Through literature search, do not see the public literature report identical with the present invention

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Weigh 10g of chitosan, 10g of sucrose and 10g of glucose as the wall material and mix evenly, add 3g (10~15% of the mass of the wall material) of water, heat to a molten state at 85°C, cool to 40°C, and add 4.5 g (15~25% of the mass of the wall material) clove essential oil, stirred at 8000r / min for 10min at high speed, then passed into a high-pressure homogenizer, homogenized three times at 70°C and a pressure of 20MPa, each time for 7min, to form an emulsion with uniform particle size , spraying and drying under the condition that the inlet temperature is 180°C, the outlet temperature is 80°C, and the atomization pressure is 0.2MPa, the microcapsule clove essential oil is obtained. The obtained microencapsulated clove essential oil is diluted 800 times with distilled water, and the diluted solution is added to the cigarette filter at 1% of the filter weight, and the filter is rolled into a cigarette, and the perfumer conducts sensory evaluation and identification. The...

Embodiment 2

[0015] Weigh 20g of chitosan, 10g of sucrose and 10g of glucose as the wall material and mix evenly, add 6g (10~15% of the mass of the wall material) of water, heat to a molten state at 95°C, cool to 30°C, and add 10g while stirring (15~25% of the mass of the wall material) clove essential oil, stirred at 10,000r / min at high speed for 10 minutes, then passed into a high-pressure homogenizer, homogenized at 80°C and a pressure of 30MPa three times, each time for 7 minutes, to form an emulsion with uniform particle size, The inlet temperature is 200°C, the outlet temperature is 100°C, and the atomization pressure is 0.5MPa, and spray drying is carried out to obtain the microcapsule clove essential oil. The obtained microcapsule clove essential oil was diluted 1000 times with distilled water, and the diluted solution was added to the cigarette filter with 3% of the filter weight, and the filter was rolled into a cigarette. The aroma increases, the aroma is soft, and harmonizes wi...

Embodiment 3

[0017] Weigh 15g of chitosan, 10g of sucrose and 15g of glucose as the wall material and mix evenly, add 4.8g (10~15% of the mass of the wall material) of water, heat at 90°C until molten, cool to 35°C, and add while stirring 8g (15~25% of the mass of the wall material) clove essential oil, stirred at 9000r / min for 10min at high speed, then passed into a high-pressure homogenizer, homogenized three times at 75°C and a pressure of 25MPa, each time for 7min, to form an emulsion with uniform particle size , spraying and drying under the condition that the inlet temperature is 190°C, the outlet temperature is 90°C, and the atomization pressure is 0.3MPa, the microcapsule clove essential oil is obtained. The obtained microcapsule clove essential oil is diluted 900 times with distilled water, and the diluted solution is added to the cigarette filter at 2% of the filter weight, and the filter is rolled into a cigarette, and the perfumer conducts sensory evaluation and identification. ...

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Abstract

The invention discloses a method for preparing microcapsule clove essential oil and application of the clove essential oil in tobacco and belongs to the technical field of cigarette processing. The method is characterized by comprising the following steps: uniformly mixing three substances, namely chitosan, sucrose and glucose which are used as wall materials at a mass ratio of (1-2):1:(1-2), adding water which accounts for 10-15wt% of three substances, heating at 85-95 DEG C until the mixture is in a molten state, cooling to 30-40 DEG C, adding clove essential oil which accounts for 15-25wt% of wall materials, carrying out high-pressure homogenization to obtain an emulsion and finally performing a spray drying technology, thereby obtaining the microcapsule clove essential oil. 100% of the clove essential oil microcapsule is dissolved in water, diluted with water, added into a cigarette filter and finally rolled into a cigarette, wherein the diluted clove essential oil microcapsule accounts for 1-3wt% of the filter. By virtue of the clove essential oil microcapsule, the influence of offensive odor in the cigarette product can be improved, the aroma quantity, aroma quality and coordination of the cigarette are greatly enriched and the smoking quality of the cigarette is improved.

Description

technical field [0001] The invention belongs to the technical field of cigarette processing, and in particular relates to a preparation method of microcapsule clove essential oil and its application in tobacco. Background technique [0002] Plants have long been a major source of natural tobacco flavors. Tobacco flavors and fragrances are specially used for flavoring and correcting various tobacco products. In the production of cigarettes, tobacco flavors and fragrances are rich in content and various in variety. Its aroma type and aroma style determine the grade and taste of tobacco products to some extent. Usually, tobacco will produce some pungent organic substances when it is burned. If some flavors are added to cigarettes, the aroma can be used to cover up the pungent taste produced during the burning process of tobacco, so that it can produce good smoke effect when smoking. However, adding essence or essential oil to shredded tobacco of cigarettes will increase the c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24D3/14
Inventor 张金芳杨存
Owner NANJING BIAOKE BIO TECH
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