Carbon black for black matrix and manufacturing method thereof
A technology of black matrix and manufacturing method, which is applied in the direction of dyeing low molecular organic compound treatment, fibrous filler, optical filter, etc., can solve problems such as poor image, achieve high contrast, realize contrast, and high insulation effect
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Embodiment 1
[0052] Preparation of dye-coated carbon black (oxidized)
[0053] 1000 g of carbon black (TPX-1099: manufactured by Cabot Co., Ltd.) was mixed with water to prepare 10 L of slurry, stirred at 95° C. for 1 hour, cooled naturally, and washed with water. This was mixed with water again to prepare 10 L of slurry, 42.9 g of 70% nitric acid was added, and it stirred at 40 degreeC for 4 hours. After cooling and washing with water, this was mixed with water again to prepare 10 L of slurry, 769.2 g of 13% sodium hypochlorite aqueous solution was added, and it stirred at 40 degreeC for 6 hours. After it was naturally cooled and washed with water, it was mixed with water again to prepare 10 L of slurry, 38.1 g of a dye (Direct Deep BLACK) with a purity of 38.4% was added, stirred at 40° C. for 1 hour, and then 10.1 g of aluminum sulfate was further added to Stir at 40°C for 1 hour. After naturally cooling this, it washed with water, filtered and dried, and obtained the carbon black fo...
Embodiment 2
[0060] Preparation of dye-coated carbon black (unoxidized)
[0061] The carbon black for black matrices of this invention was obtained by performing substantially the same process as Example 1 except not carrying out oxidation process with nitric acid and sodium hypochlorite aqueous solution. The carboxyl group content of the obtained dye-coated carbon black was 3.4 mmol / g.
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