Method for processing wastes generated during butyl butyryl lactate production process
A technology of butyl butyryl lactate and a treatment method, which is applied in the separation/purification of carboxylate, preparation of carboxylate, chemical instruments and methods, etc., can solve problems such as insoluble in water and glycerol, waste, environmental pollution and the like , to achieve the effect of improving the comprehensive utilization rate of resources, the method is reasonable, and the processing method is simple
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[0023] A kind of processing method of the waste that produces in the butyl butyryl lactate production, method step is as follows:
[0024] (1) Treatment of the former fraction
[0025] 1) Select a fractionating tower with efficient separation function, and pump the mixed solution of butyric acid, butyl lactate and butyl butyryl lactate in the preceding fraction into the fractionating tower;
[0026] 2) depressurize the fractionating tower to 20mmhg, start heating;
[0027] 3) When the temperature is 73°C, the reflux ratio is set to 1:2, and the butyric acid component is collected. When the temperature reaches 80°C, the reflux ratio is changed to 12:1, and the butyric acid collection ends;
[0028] 4) When the temperature is 82°C, the reflux ratio is set to 1:2, and the butyl lactate component is collected. When the temperature reaches 102°C, the reflux ratio is changed to 12:1, and the butyl lactate collection ends;
[0029] 5) When the temperature is 107°C, the reflux ratio...
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