Co-production preparation method of ceramide and glucoside (lipoyl) sphingosine
A technology of ceramide and sphingosine is applied in the preparation of sugar derivatives, chemical instruments and methods, separation/purification of carboxylic acid amides, etc. The effect of improving the comprehensive utilization rate of resources and improving the prospect of industrial application
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Embodiment 1
[0027] Embodiment 1 uses konjac flying powder as raw material coproduction to prepare ceramide and glucoside (fat) ceramide
[0028] Get 1000 grams of by-product konjac flying powder in the processing of konjac fine powder, use 6 times the amount of 80% ethanol to stir and heat to extract three times and filter (the filter cake can be used for making feed through drying), merge three extractions, add milk of lime to adjust the pH value to 10.0, a large amount of fatty acid calcium precipitates, let it stand for 3-5 hours, filter out the fatty acid calcium, adjust the pH of the filtrate to 5.0 with hydrochloric acid (concentrated hydrochloric acid is diluted with water at a volume ratio of 1:1), concentrate and recover ethanol until it has no alcohol smell, Add an equal volume of water to the concentrated solution to obtain a solution, and then use petroleum ether / methanol / glacial acetic acid mixed organic solvent to carry out fractional extraction, and the volume ratio of petro...
Embodiment 2
[0029] Example 2 Co-production of ceramide and glucoside (fat) ceramide with rice bran residue as raw material
[0030] Get 1000 grams of rice bran residue after rice oil processing, stir and heat extraction three times with 8 times the amount of 90% ethanol and filter (the filter cake can be used to make feed after drying), combine three extractions, add milk of lime to adjust the pH value to 10.0, resulting in a large amount of Fatty acid calcium precipitates, let it stand for 2-4 hours, filter to remove fatty acid calcium, adjust the pH of the filtrate to 5.0 with hydrochloric acid (concentrated hydrochloric acid is diluted with water at a volume ratio of 1:1), concentrate and recover ethanol until there is no alcohol smell, and add to the concentrated solution 1.5 times the volume of water to obtain a solution, and then use dichloromethane / methanol / glacial acetic acid mixed organic solvent to carry out fractional extraction, and the volume ratio of dichloromethane / methanol / ...
Embodiment 3
[0031] Example 3 Co-production of ceramide and glucoside (fat) ceramide with konjac powder as raw material
[0032] Get 1000 grams of by-product konjac flying powder in the processing of konjac fine powder, use 4 times the amount of 95% ethanol to stir and heat to extract three times and filter (the filter cake can be used for making feed through drying), merge three extractions, add milk of lime to adjust the pH value to 11.0, a large amount of fatty acid calcium precipitates, let it stand for 6-8 hours, filter out the fatty acid calcium, adjust the pH of the filtrate to 6.0 with 2M sulfuric acid, concentrate and recover ethanol until there is no alcohol smell, add 2 times the volume of water to the concentrated solution, and obtain a solution , and then use the mixed organic solvent of cyclohexane / methanol / glacial acetic acid to carry out fractional extraction, and the volume ratio of cyclohexane / methanol / glacial acetic acid is 10:1:0.1, 10:2:0.3, 10:3:0.6 , 10:4:0.8, 10:5:1.0...
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