composite material
A technology of composite materials and composite particles, applied in the direction of heterogeneous insulating materials, synthetic resin layered products, aircraft electrostatic dischargers, etc., can solve the problems of reducing the overall conductivity of composite materials and structures
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example 1
[0109] Preparation of nickel-based conductive composite particles
[0110] In a twin-screw extruder (Sumikaexel 5003P from Sumitomo), through a melt-mixing process, filamentous nickel (Ni) flakes (525 nickel purchased from Novamant) in an amount sufficient to obtain a final concentration of 70% by weight Powder) dispersed in functionalized polyethersulfone (PES) polymer. A pure sample of the same PES polymer was used as a control. Use a high-shear screw profile that maximizes the dispersion level. The profile includes a conventional mixing section combined with a random mixing unit to create the best balance between shear and pressure in the extruder barrel. The temperature profile and process conditions used are reported in Table 1.
[0111] Table 1. Dispersion conditions of composite nickel / PES blend
[0112]
[0113] An Alpine cryogenic grinding system equipped with different rotating grinding media is used to cryogenically grind the resulting Ni / PES blend to produce micron-si...
example 2
[0115] The effect of nickel-based conductive particles on the electrical properties of composite structures
[0116] The composite nickel / PES particles of Example 1 were dispersed in Cytec Engineered Materials Ltd (UK) provided by the spraying process. 977-2-34%-194-IMS24K unidirectional tape (unidirectional carbon fiber impregnated with epoxy-based matrix) on the surface. The particle loading is 10% by volume based on the total resin volume in the strip. Laying a plurality of the strips on top of each other, and placing particles between adjacent strips to form a 1.5 mm thick quasi-isotropic test plate. The board was then cured in an autoclave at 180°C according to a 2 hour curing cycle. Mark this test board as "2A".
[0117] During the curing process, the particles are placed in the resin-rich area between adjacent carbon fiber layers that define the interlayer area. The thermoplastic component of the composite particles dissolves in the epoxy-based matrix of the strip during...
example 3
[0123] Effect of particle loading between conductive layers on the mechanical properties of composite structures
[0124] The same composite Ni / PES particles used in Example 2 with two different loadings (10% by volume and 20% by volume) were dispersed in a product from Cytec Engineering Materials, UK. 977-2-34%-194-IMS24K unidirectional strip on the surface. Two test plates with different particle loads are formed by laying down strips with particles dispersed on it. The resulting test panels are evaluated to determine the effect of composite particles on thermomechanical properties. The test plate containing 10% particles is marked as "3B" and the test plate containing 20% particles is marked as "3C". For comparison purposes, a similar test plate without composite Ni / PES particles was manufactured and marked as "Reference 2".
[0125] The mechanical properties of the test board are shown in Table 3.
[0126] Table 3. Composites of inserted particles and corresponding mechanic...
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