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Treatment process for degumming and bleaching silk

A treatment process, silk degumming technology, applied in the field of dyeing and finishing process, can solve the problems of damage to skin, clothes and equipment, volatile irritating smell, reduce the strength and elongation of silk fiber, etc., to reduce the action time, accelerate penetration and effect , The effect of reducing the number of washings

Active Publication Date: 2015-02-11
HUZHOU NEW ZHONGHU KNITTED CLOTHING MAKING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Alkali degumming is easy to damage silk fibroin and reduce the strength and elongation of silk fibers; acid degumming is not easy to control, the cost is high, and there is a volatile irritating smell in production, which can damage skin, clothes and equipment, and is rarely used in production.
The enzymatic degumming method is superior to the traditional acid and alkali bath boiling degumming method in reducing gray damage, and its degumming quality is better than that of the soap-alkali method. It is technically simple and easy to operate, and the enzyme is a natural protein, which is easy to biodegrade. Easy to handle and good for environmental protection, but the high cost is the main reason why it cannot be widely used

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Selected material: mulberry silk.

[0021] The treatment process of present embodiment mulberry silk degumming, bleaching, specifically as follows:

[0022] (1) Pretreatment: first put the silk into an airtight container, feed 20g / L active oxygen to carry out pretreatment to the silk;

[0023] (2) Preliminary training: prepare the preliminary training liquid (the formula of the preliminary training liquid is: soda ash 0.3g / l, sodium silicate 2g / l, industrial soap 0.3g / l and hydrosulfite 0.3g / l), the pretreated Put the silk into the initial refining solution, turn it up and down for 3 minutes, and after 20 minutes of treatment, take out the silk, add the specified amount of hydrosulfite, stir well to dissolve, put in the silk and turn it up and down for 1 minute, and continue to process for 40 minutes;

[0024] (3) Re-training: prepare re-training liquid (the formula of re-training liquid is: soda ash 0.4g / l, sodium silicate 0.6g / l, hydrosulfite 0.3g / l and dispersant WA...

Embodiment 2

[0035] Material selection: tussah silk.

[0036] The treatment process of tussah silk degumming and bleaching in this embodiment is as follows:

[0037] (1) Pretreatment: first silk is put into airtight container, feeds the active oxygen of 35g / L to carry out pretreatment to silk;

[0038] (2) Preliminary training: prepare the preliminary training liquid (the formula of the preliminary training liquid is: soda ash 0.3g / l, sodium silicate 2g / l, industrial soap 0.3g / l and hydrosulfite 0.3g / l), the pretreated Put the silk into the initial training solution, turn it up and down for 3 minutes, and after 30 minutes of treatment, take out the silk, add the specified amount of hydrosulfite, stir to dissolve, put in the silk and turn it up and down for 5 minutes, and continue to process for 10 minutes;

[0039] (3) Re-training: prepare re-training liquid (the formula of re-training liquid is: soda ash 0.4g / l, sodium silicate 0.6g / l, hydrosulfite 0.3g / l and dispersant WA1.5g / l). Put t...

Embodiment 3

[0050] Selected material: silkworm silk.

[0051] The treatment process of silk degumming and bleaching in this embodiment is as follows:

[0052](1) Pretreatment: first put the silk into an airtight container, feed 50g / L active oxygen to carry out pretreatment to the silk;

[0053] (2) Preliminary training: prepare the preliminary training liquid (the formula of the preliminary training liquid is: soda ash 0.3g / l, sodium silicate 2g / l, industrial soap 0.3g / l and hydrosulfite 0.3g / l), the pretreated Put the silk into the initial training solution, turn it up and down for 1 minute, and after 25 minutes of treatment, take out the silk, add the specified amount of hydrosulfite, stir well to dissolve, put in the silk and turn it up and down for 3 minutes, and continue to process for 30 minutes;

[0054] (3) Re-training: prepare re-training liquid (the formula of re-training liquid is: soda ash 0.4g / l, sodium silicate 0.6g / l, hydrosulfite 0.3g / l and dispersant WA1.5g / l.), the Put...

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PUM

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Abstract

The invention discloses a treatment process for degumming and bleaching silk. The treatment process comprises the following steps: carrying out pretreatment, namely firstly putting the silk into a closed container, introducing 20-50g / L active oxygen for carrying out the pretreatment on the silk; and then carrying out treatment of primary refining, secondary refining, bleaching, washing with water, and shaping. The treatment process disclosed by the invention has the beneficial effects that at the pretreatment stage, the silk is put in the closed container, the 20-50g / L active oxygen is introduced for carrying out the pretreatment on the silk, macromolecular chains of silk glue can be broken, and a silk-glue layer is cracked and loose, so that the permeation and the action of primary-refining liquid and secondary-refining liquid in the next procedure are accelerated, the action time is reduced, and the used amount of the primary-refining liquid and the secondary-refining liquid is reduced. The treatment process disclosed by the invention has the advantages that a water resource is saved, the used amount of chemicals is reduced, and the environment pollution is reduced.

Description

technical field [0001] The invention belongs to the dyeing and finishing process in the textile industry, in particular to the degumming and bleaching process of silk. Background technique [0002] Silk is the fiber that solidifies after the silk liquid in the silkworm body is spouted out, and is called cocoon silk. It is composed of two silk proteins (also known as silk fibroin) with a nearly triangular or semi-elliptical cross-section wrapped in sericin, as well as pigments, oil waxes and inorganic substances, which are present in the sericin. Among them, sericin has a certain protective effect on silk fibroin, but if the content is too much, it will affect the luster and feel of silk fibroin and the process of silk fiber processing, while impurities such as oil and wax will bring certain difficulties to post-processing. . Therefore, before dyeing and finishing, most of the sericin, grease, wax and other sundries must be removed to make the silk fiber soft, loose and cle...

Claims

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Application Information

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IPC IPC(8): D06L3/02D06L1/16D01C3/02D06M11/76D06M11/79D06M11/32D06M101/10D06L4/13
Inventor 闵滢春
Owner HUZHOU NEW ZHONGHU KNITTED CLOTHING MAKING
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