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Tube and tube reactor

A shell-and-tube reactor and the technology of the reactor are applied in the field of reactors and can solve the problems of affecting the safety of the reactor, the problem of affecting the reaction performance of the chemical production process, and the difficulty of heat transfer to the outside world.

Active Publication Date: 2016-07-20
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In practice, it has been found that even for newly loaded reactors, the pressure drop of the vertical shell-and-tube catalytic reactor is relatively high, and there is a lot of room for improvement in the industrial effect of the reactor.
[0006] In addition, in terms of heat transfer, if high-pressure water and steam are used to obtain heat, due to the influence of the lower tube wall, a large-area gas film will be formed on the outer surface of the vertical tubes, that is, the problem of gas attachment.
As a result, the heat is not easily transmitted, which will eventually not only affect the reaction performance of the chemical production process, but also affect the safety of the reactor

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0060] Example 1. Select a stainless steel tube with a length of 10 m and an inner diameter of 5.15 cm in a tube-and-tube reactor, and make it an included angle of 30° with the horizontal direction during the reaction.

Embodiment 2

[0061] Example 2. Select a stainless steel tube with a length of 10 m and an inner diameter of 5.15 cm in the tube-and-tube reactor, and make it have an included angle of 45° with the horizontal direction during the reaction.

Embodiment 3

[0062] Example 3. In the shell-and-tube reactor, a stainless steel shell-and-tube tube with a length of 10 m and an inner diameter of 5.15 cm was selected, and during the reaction, it had an included angle of 60° with the horizontal.

[0063] Wherein, the method of tilting the tubes in Examples 1-3 can be realized by using the reactor provided by the present invention or by using the assembling method provided by the present invention. The obtained reaction results are listed in Table 1, and it can be seen that the present invention The advantage in reducing the pressure drop across the reaction apparatus is obvious.

[0064] Table 1

[0065]

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PUM

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Abstract

The invention discloses a tubular reactor which comprises a reactor cabinet and a plurality of tubulations arranged in the reactor cabinet at intervals, wherein the reactor cabinet comprises a cabinet body and a horizontal base fixed at the bottom of the cabinet body, and the reactor cabinet is also provided with a reaction material inlet and a reaction product output which are communicated with the plurality of tubulations, wherein at least one tubulation is obliquely arranged relative to the horizontal base. As at least one tubulation in the tubular reactor provided by the invention is obliquely arranged relative to the horizontal base, in the process of filling catalyst, the catalyst can slowly slide in the tubulations with the help of the weight of the catalyst relatively, so that the uniformity of catalyst filler can be provided, the fluidity of the reaction fluid can be improved, the pressure drop can be reduced, the problem of gas attachment generated in the operation of exothermic reaction can be solved, and the heat transfer of the tubulations can be improved, and then the security and reliability of the reactor can be ensured.

Description

technical field [0001] The present invention relates to the field of reactors, in particular to a shell and tube type reactor, and more particularly to a shell and tube type fixed bed catalytic reactor. Background technique [0002] In the chemical industry, a fixed bed reactor refers to a device in which a fluid passes through a fixed bed formed by a solid catalyst to carry out chemical reactions. Fixed bed catalytic reactors are widely used in industrial production, for example, ammonia synthesis, distillate hydrogenation, residue hydrogenation. However, for chemical processes with large heat release, such as FT synthesis, aniline hydrogenation to cyclohexylamine, ethylene oxidation to ethylene oxide, sulfur dioxide oxidation to sulfur trioxide, synthesis gas to methanol, acetylene chlorination to vinyl chloride, benzene Oxidation to maleic anhydride, o-xylene to phthalic anhydride, etc., in order to facilitate heat extraction and stable control during the reaction proces...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/06
CPCB01J8/008B01J8/06
Inventor 侯朝鹏夏国富孙霞王奎吴玉晋超阎振楠李明丰徐润胡志海聂红石亚华李大东
Owner CHINA PETROLEUM & CHEM CORP