Soft-magnetic magnetostrictive ferrite material and manufacturing method thereof
A ferrite material and magnetostriction technology, applied in the field of magnetic materials, to achieve the effect of both market competitiveness, high reliability, and negative magnetostriction coefficient
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Embodiment 1
[0022] Proportion the main components and additives in specified amounts as shown in Table 1.
[0023] The preparation method is:
[0024] (1) Primary ball milling: the main components are mixed according to the ratio, and the obtained mixture is wet-processed primary ball milling, and the average particle size of the granular material after the primary ball milling is 0.8-1.5 μm.
[0025] (2) Pre-burning: Pre-burning the pellets after primary ball milling in the air, the pre-burning temperature is controlled at 1050° C., and kept for 4 hours.
[0026] (3) Secondary ball milling: perform wet secondary ball milling on the calcined granules together with the additives, and the average particle size of the granules after the secondary ball milling is 0.8-1.2 μm.
[0027] (4) Molding and sintering: dry the granules after secondary ball milling, add a polyvinyl alcohol solution with a concentration of 12% of 11wt% of pre-fired material, mix evenly, spray granulate, and press to fo...
Embodiment 2
[0038] The main components and additives are proportioned according to the specified amounts shown in Table 2.
[0039] The preparation method is:
[0040] (1) Primary ball milling: the main components are mixed according to the ratio, and the obtained mixture is wet-processed primary ball milling, and the average particle size of the granular material after the primary ball milling is 0.8-1.5 μm.
[0041] (2) Pre-burning: Pre-burn the pellets after primary ball milling in the air, the pre-burning temperature is controlled at 1050° C., and the temperature is kept for 0.5 hours.
[0042] (3) Secondary ball milling: perform wet secondary ball milling on the calcined granules together with the additives, and the average particle size of the granules after the secondary ball milling is 0.8-1.2 μm.
[0043] (4) Molding and sintering: dry the granules after the secondary ball milling, add a polyvinyl alcohol solution with a concentration of 10wt% of 13wt% of the weight of the pre-fir...
Embodiment 3
[0054] The main components and additives were mixed in predetermined amounts as shown in Table 3.
[0055] The preparation method is:
[0056] (1) Primary ball milling: the main components are mixed according to the ratio, and the obtained mixture is wet-processed primary ball milling, and the average particle size of the granular material after the primary ball milling is 0.8-1.5 μm.
[0057] (2) Pre-burning: Pre-burn the pellets after primary ball milling in the air, the pre-burning temperature is controlled at 1110° C., and the temperature is kept for 2.5 hours.
[0058] (3) Secondary ball milling: perform wet secondary ball milling on the calcined granules together with the auxiliary components, and the average particle size of the granules after the secondary ball milling is 0.8-1.2 μm.
[0059] (4) Molding and sintering: dry the granules after secondary ball milling, add a polyvinyl alcohol solution with a concentration of 12wt% of the weight of pre-sintered material, m...
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