Polyurethane acrylate sealant and preparation method thereof
A polyurethane acrylate and sealant technology, applied in polyurea/polyurethane adhesives, adhesives, adhesive types, etc., can solve problems such as poor adhesion, unsatisfactory use requirements, and unreasonable formula ratios, etc., to achieve The effect of good adhesion, reasonable proportion and simple preparation process
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Embodiment 1
[0037] The polyurethane acrylate sealant of the present invention is made up of following components by weight:
[0038]
[0039]
[0040] The preparation method comprises the following steps:
[0041] A. Preparation of polyurethane prepolymer
[0042] Using a quantitative feeding device, add biuret polyisocyanate and polyether polyol in the reaction device at a mass ratio of 25:1, close the reaction device, stir, vacuumize and reduce pressure, and react at 40°C for 0.5 hours;
[0043] B. Preparation of polyurethane acrylate sealant
[0044] Add isooctyl acrylate, glycidyl methacrylate, isobutyl methacrylate, and vinyl acetate to the reaction device, stir and control the temperature of the reactor at 60°C, add tackifier and adhesion promoter, and use Cool the cooling device down to 30°C, add plasticizer, disperse evenly, filter through the filter device, and then use the automatic filling device to fill and store.
[0045] The reaction device 1 described in the presen...
Embodiment 2
[0061] The polyurethane acrylate sealant of the present invention is made up of following components by weight:
[0062]
[0063] The preparation method comprises the following steps:
[0064] C. Preparation of polyurethane prepolymer
[0065] Using a quantitative feeding device, add biuret polyisocyanate and polyether polyol in the reaction device at a mass ratio of 25:1, close the reaction device, stir, vacuumize and reduce pressure, and react at 40°C for 0.5 hours;
[0066] D. Preparation of polyurethane acrylate sealant
[0067] Add isooctyl acrylate, glycidyl methacrylate, isobutyl methacrylate, and vinyl acetate to the reaction device, stir and control the temperature of the reactor at 60°C, add tackifier and adhesion promoter, and use Cool the cooling device down to 30°C, add plasticizer, disperse evenly, filter through the filter device, and then use the automatic filling device to fill and store.
[0068] The quantitative feeding device reaction device, cooling ...
Embodiment 3
[0070] The polyurethane acrylate sealant of the present invention is made up of following components by weight:
[0071]
[0072] The preparation method comprises the following steps:
[0073] A. Preparation of polyurethane prepolymer
[0074] Using a quantitative feeding device, add biuret polyisocyanate and polyether polyol in the reaction device in a mass ratio of 1, close the reaction device, stir, vacuumize and reduce pressure, and react at 100 ° C for 3 hours;
[0075] B. Preparation of polyurethane acrylate sealant
[0076] Add isooctyl acrylate, glycidyl methacrylate, isobutyl methacrylate, and vinyl acetate to the reaction device, stir and control the temperature of the reactor at 80°C, add tackifier and adhesion promoter, and use The cooling device cools down to 50°C, add plasticizer, disperse evenly, filter through the filter device, and then use the automatic filling device to fill and store.
[0077] The quantitative feeding device reaction device, cooling d...
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