Magnetic carrier and two-component developer
A technology of magnetic carrier and magnetic substance, applied in developing agent, electro-recording technique, optics, etc., can solve problems such as inability to improve developing performance
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[0259] Next, the present invention will be described more specifically by means of preparation examples and examples below, which shall not be construed as limiting the present invention.
[0260] [Preparation of Magnetic Substance 1]
[0261] Fe 2+ (1.5 mol / L) ferrous sulfate aqueous solution (26.7L) and containing Si 4+ (0.2 mol / L) sodium silicate (No.3) aqueous solution (1.0 L) was added to 3.4 mol / L sodium hydroxide aqueous solution (22.3 L), the pH was controlled to 6.8 and the temperature was raised to 90°C. Furthermore, a 3.5 mol / L sodium hydroxide aqueous solution (1.2 L) was added, and the pH was controlled to be 8.5. Stirring was continued and air was supplied at a rate of 100 L / min for 90 minutes instead of gas. The mixed solution was neutralized to pH 7 with dilute sulfuric acid. The resulting particles were washed with water, filtered, dried and pulverized to obtain magnetite, ie, magnetic substance 1 .
[0262] Magnetic substance 1 (spherical magnetite, numb...
preparation example
[0315] ・Polyester resin 1:80 parts by mass
[0316] ・Polyester resin 2: 20 parts by mass
[0317] · Paraffin (melting point: 75°C): 7 parts by mass
[0318] Cyan pigment (C.I. Pigment Blue 15:3): 7 parts by mass
[0319] 3,5-di-tert-butylbutyl salicylate aluminum compound: 1 part by mass
[0320] The above-mentioned materials were mixed well by a Henschel mixer (FM-75 type, manufactured by Nippon Coke Engineering Co., Ltd.) and passed through a biaxial kneader (PCM-30 type, manufactured by IKEGAI) set at a temperature of 130° C. kneading. The obtained kneaded product was cooled, and coarsely pulverized by a hammer mill into particles having a size of 1 mm or less to obtain a crude product. The obtained crude product was finely pulverized by a collision jet mill using high-pressure gas.
[0321] Next, the obtained finely pulverized product was classified by a wind classifier (Elbow-jet, LABO EJ-L3, manufactured by Nittetsu Mining Co., Ltd.) using the Coanda effect to simul...
Embodiment 1
[0335] To Magnetic Carrier 1 (92 parts by mass), Toner 1 (8 parts by mass) was added. The mixture was stirred by a V-shaped mixer (V-20, manufactured by Seishin Enterprise Co., Ltd.), whereby a two-component system developer shown in Table 5 was obtained.
[0336] Using a modified machine of image RUNNER ADVANCE C5030, a multifunction machine for digital office manufactured by Cannon Inc., as an image forming apparatus, a two-component system developer was supplied to a developing apparatus for cyan, and toner 1 was supplied to Refill bottle for cyan. Images were formed and evaluated as follows. Note that the image forming apparatus operates by combining a rectangular AC voltage (frequency is 8.0 kHz, Vpp is 0.7 kV) and a DC voltage V DC Applied to the developer carrying member and reformed by closing the developer discharge port of the developing container. When evaluating images after long-term repeated use, control the DC voltage V of the developer carrying member DC , ...
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