Food antioxidant preservative and preparing method thereof
A preservative and food technology, which is applied in the field of food additives, can solve the problems of light and heat instability, high heavy metal content, and weak anti-oxidation, and achieve no toxic side effects, strong complexation, and strong anti-oxidation Effect
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Embodiment 1
[0026] Weigh 100 parts of gallnut, 30 parts of sulfuric acid, 35 parts of glucose, 10 parts of rice bran, 15 parts of wheat bran, 25 parts of Aspergillus niger, 5 parts of n-propanol, 50 parts of lime, 20 parts of p-toluenesulfonic acid , 60 parts of water, 55 parts of calcium magnesium phytate, 40 parts of cyclohexyl alcohol, 45 parts of inorganic phosphoric acid, and 10 parts of cyclohexanethiol.
[0027] Put gallnuts, glucose, rice bran and wheat bran into the reaction kettle, stir evenly, add sulfuric acid and Aspergillus niger, stir for 10 minutes, add n-propanol and p-toluenesulfonic acid, heat up to 30°C, and stir for 20 minutes.
[0028] Add calcium magnesium phytate, cyclohexyl alcohol and inorganic phosphoric acid, react for 30 minutes, add water and the remaining materials, react for 40 minutes, esterify and transposition refining.
[0029] The melting point of the product is 180°C, the residue on ignition is 0.1%, the content of arsenic salt is 0.0003%, the content...
Embodiment 2
[0031] Weigh 100 parts of gallnut, 50 parts of sulfuric acid, 55 parts of glucose, 30 parts of rice bran, 35 parts of wheat bran, 45 parts of Aspergillus niger, 25 parts of n-propanol, 70 parts of lime, 40 parts of p-toluenesulfonic acid , 80 parts of water, 75 parts of calcium magnesium phytate, 60 parts of cyclohexyl alcohol, 65 parts of inorganic phosphoric acid, and 50 parts of cyclohexanethiol.
[0032] Put gallnuts, glucose, rice bran and wheat bran into the reaction kettle, stir evenly, add sulfuric acid and Aspergillus niger, stir for 30 minutes, add n-propanol and p-toluenesulfonic acid, heat up to 50°C, and stir for 40 minutes.
[0033] Add calcium magnesium phytate, cyclohexanehexanol and inorganic phosphoric acid, react for 50 minutes, add water and the remaining materials, react for 60 minutes, esterify and transposition refining.
[0034] The melting point of the product is 190°C, the residue on ignition is 0.08%, the content of arsenic salt is 0.00025%, the cont...
Embodiment 3
[0036] Weigh 100 parts of gallnut, 35 parts of sulfuric acid, 40 parts of glucose, 15 parts of rice bran, 20 parts of wheat bran, 30 parts of Aspergillus niger, 10 parts of n-propanol, 55 parts of lime, 25 parts of p-toluenesulfonic acid , 65 parts of water, 60 parts of calcium magnesium phytate, 45 parts of cyclohexyl alcohol, 50 parts of inorganic phosphoric acid, 20 parts of n-propyl 3,4,5-trihydroxybenzoate.
[0037]Put gallnuts, glucose, rice bran and wheat bran into the reaction kettle, stir evenly, add sulfuric acid and Aspergillus niger, stir for 15 minutes, add n-propanol and p-toluenesulfonic acid, heat up to 35°C, and stir for 25 minutes.
[0038] Add calcium magnesium phytate, cyclohexanehexanol and inorganic phosphoric acid, react for 35 minutes, add water and remaining materials, react for 45 minutes, esterify and transposition refining.
[0039] The melting point of the product is 200°C, the residue on ignition is 0.05%, the content of arsenic salt is 0.0002%, t...
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