Magnetic field and application of magnetic nanowires in transparent conductive film as well as transparent conductive film and preparation method
A transparent conductive film, magnetic nanotechnology, applied in conductive materials, conductive materials, cable/conductor manufacturing, etc., can solve the problems of high film preparation cost and limitations, and achieve the purpose of improving conductivity and light transmittance, and improving experimental technology. Effect
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Embodiment 1
[0036] 0.86 g ferrous chloride FeCl 2 and 2.00 g ferric chloride FeCl 3 Dissolve in 10 mL deionized water, heat to 80 oC under the protection of nitrogen, then dissolve 0.58 g C 6 h 8 o 7 ·H 2 NH of O 3 ·H 2 O solution was added dropwise to the above iron salt solution, so that the pH value of the iron salt gradually increased until the pH value of the solution was equal to 9, about 6 mL NH 3 ·H 2 O, and then raise the temperature to 180oC for about 2 hours to obtain iron oxide Fe 3 o 4 suspension.
[0037] The alumina template required for the preparation of magnetic nanowires was prepared by one oxidation method. First, the aluminum foil with a purity of 99.999% was pretreated, immersed in acetone for 24 hours to remove surface oil, then annealed at 500 oC in air for 6 hours to relieve the internal stress of the aluminum sheet, and then chemically polished to a mirror surface in a mixed acid solution degree. A 40 V regulated DC power supply was used for anodizing...
Embodiment 2
[0040] 2.70 g NiSO 4 ·6H 2 O and 0.40 g NiCl 2 Dissolve in 10 mL deionized water, heat to 80 oC under nitrogen protection, and then dissolve 0.40 g H 3 BO 3 NH 3 ·H 2O solution was added dropwise to the above nickel salt solution, so that the pH value of the nickel salt gradually increased until the pH value of the solution was equal to 4, about 3 mL NH 3 ·H 2 O, and then raise the temperature to 180oC for about 2 h to obtain a nickel oxide suspension.
[0041] An oxidation method is used to prepare alumina templates required for magnetic nanowires. First, the aluminum foil with a purity of 99.999% was pretreated, immersed in acetone for 24 hours to remove surface oil, then annealed at 500 oC in air for 6 hours to relieve the internal stress of the aluminum sheet, and then chemically polished to a mirror surface in a mixed acid solution degree. A 40 V regulated DC power supply was used for anodizing, the aluminum sheet was used as the working electrode, the steel plat...
Embodiment 3
[0044] 2.52 g CoSO 4 ·7H 2 O and 0.07 g NaCl were dissolved in 10 mL deionized water, heated to 80 oC under the protection of nitrogen, and then dissolved with 0.50 g H 3 BO 3 NH 3 ·H 2 O solution was added dropwise to the above cobalt salt solution, so that the pH value of the cobalt salt gradually increased until the pH value of the solution was equal to 5, about 4 mL NH 3 ·H 2 O, and then raise the temperature to 180oC for about 2 h to obtain cobalt oxide suspension.
[0045] An oxidation method is used to prepare alumina templates required for magnetic nanowires. First, the aluminum foil with a purity of 99.999% was pretreated, immersed in acetone for 24 hours to remove surface oil, then annealed at 500 oC in air for 6 hours to relieve the internal stress of the aluminum sheet, and then chemically polished to a mirror surface in a mixed acid solution degree. A 40 V regulated DC power supply was used for anodizing, the aluminum sheet was used as the working electrod...
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