Polyvinyl chloride Grade-A flame-retardant fireproof wear-resistant wood-plastic floor material
A technology of polyvinyl chloride and wood-plastic flooring, applied in the field of interior decoration materials, can solve the problems of improving the fire protection level, etc., and achieve the effects of good compression creep resistance, good dimensional stability and low price
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Embodiment 1
[0048] The preparation of embodiment 1 flame-retardant polyether
[0049] A cylindrical airtight reaction vessel with a height of 2 meters, an arc generator is arranged in the reaction vessel, and a microwave generator is arranged at a height of 1.5m on the wall of the reactor. Before the reaction starts, the container is filled with nitrogen and carbon dioxide (volume ratio 100:1.5) after vacuuming, so that the pressure in the container is 75MPa.
[0050] The catalyst is a mixture of 0.6 parts by mass of methanol, 0.5 parts by mass of silicone oil, 0.3 parts by mass of sodium silicate, and 0.1 parts by mass of sodium bicarbonate.
[0051] Rare earth fluoride (purchased from Yixing Xinweilicheng Rare Earth Co., Ltd., 2000 mesh) with mass parts of 1, 0.5, 1.5, and 1.5, butylene oxide, catalyst, and polytetrafluoroethylene at a temperature of 560 ° C and a pressure It is obtained after 3 hours of reaction under the reaction conditions of 75MPa, voltage of 15,000 volts, and micr...
Embodiment 2
[0052] Preparation of embodiment 2 flame retardant polyether
[0053] Equipment and pressure control are the same as in Example 1.
[0054] The catalyst is a mixture of 0.7 parts by mass of methanol, 0.6 parts by mass of silicone oil, 0.5 parts by mass of sodium silicate, and 0.2 parts by mass of sodium bicarbonate.
[0055] Rare earth fluoride (purchased from Yixing Xinweilicheng Rare Earth Co., Ltd., 2000 mesh) with mass parts of 1, 0.5, 2.0, and 1.5, butylene oxide, catalyst, and polytetrafluoroethylene at a temperature of 550 ° C and a pressure It is obtained after 3 hours of reaction under the reaction conditions of 75MPa, voltage of 15,000 volts, and microwave frequency of 100GHz.
Embodiment 3
[0056] The preparation of embodiment 3 flame-retardant polyether
[0057] Equipment and pressure control are the same as in Example 1.
[0058] Catalyst is with embodiment 2. The mass parts are respectively 1, 0.5, 2.0, 1.5 lanthanum fluoride (purchased from Yixing Xinweilicheng Rare Earth Co., Ltd.), butylene oxide, catalyst, and polytetrafluoroethylene at a temperature of 550 ° C and a pressure of 75 MPa. Under the reaction conditions of a voltage of 15,000 volts and a microwave frequency of 100 GHz, it was obtained after 3 hours of reaction.
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