Disperse dye compound as well as preparation method and application thereof
A technology of disperse dyes and compounds, applied in acylation preparation, dyeing method, organic chemistry, etc., can solve the problems of low tinting strength, low affinity, easy entry and exit, etc., to improve affinity, increase van der Waals force, and increase contact face effect
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[0025] Add 2.09g of purified and vacuum-dried C.I. Disperse Red 13 dye to a 1000ml three-necked flask, add an appropriate amount of dehydrated 600ml of dichloromethane as a solvent, stir to completely dissolve the disperse dye, add 1.21g and undergo dehydration treatment Accurately weigh 0.79g of diformyl chloride compound, dissolve and dilute it with an appropriate amount of reaction solvent, slowly drop it into a stirred reactor in an ice bath, and react at room temperature for 2-4h. Thin-layer sampling was followed to track the reaction process. After the reaction was completed, 100ml of dilute acid solution was added, extracted and separated, the dye solution was rotary evaporated to remove the dichloromethane solvent, and then washed and filtered with an appropriate amount of sodium carbonate solution, and washed with water to obtain 2.32g of the crude product. The rate is 80.56%.
[0026] The crude product is recrystallized from dimethylformamide to obtain the pure produ...
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