Special single-component jointing and gap filling silicon rubber for curing EMAS at room temperature and preparation method of special single-component jointing and gap filling silicon rubber
A room temperature curing, one-component technology, applied in the field of silicone rubber, can solve the problems of not being able to meet the EMAS system, poor natural aging resistance, and difficult repairs, and achieve unaffected flame retardancy, low thickening, and excellent reinforcement effect of effect
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Embodiment 1
[0034] Select 90 parts of α, ω-dihydroxypolydimethylsiloxane (molecular weight 70000, produced by Shin-Etsu Japan), 1 part of linear polydimethylsiloxane with hydroxyl end group (molecular weight 10000, produced by Dow Corning), and after three 5 parts of fumed silica pretreated by functional siloxane and hexamethyldisilazane, 10 parts of aluminum hydroxide pretreated by trifunctional siloxane and D4, 15 parts of melamine cyanurate , mix evenly in the kneader, transfer the rubber material to a three-roll machine for grinding, and then transfer it to the kneader to heat up and stir, keep the temperature of the rubber material at 100°C, and vacuum degree ≥ 0.085Mpa, stir and vacuum dry 2 hours. figure 1 It is a flowchart of the drying of the sizing material of the present invention. Such as figure 1 The specific steps of rubber drying in the actual production process can be obtained.
[0035] Put the dried rubber material into the planetary stirring tank, and when the sealing t...
Embodiment 2
[0037] Select 110 parts of α, ω-dihydroxypolydimethylsiloxane (molecular weight 70000, produced by Shin-Etsu, Japan), and 5 parts of linear polydimethylsiloxane (molecular weight 10000, produced by Dow Corning) whose terminal groups are hydroxyl groups. 10 parts of fumed silica pretreated by functional siloxane and hexamethyldisilazane, 20 parts of aluminum hydroxide pretreated by trifunctional siloxane and D4, 10 parts of melamine cyanurate Mix evenly in the kneader, transfer the rubber material to the three-roll machine for grinding, and then transfer it to the kneader to heat up and stir, keep the temperature of the rubber material at 120°C, and the vacuum degree ≥ 0.095Mpa, stir and evacuate Let dry for 3 hours.
[0038] Put the dried rubber into the planetary stirring tank. When the sealed temperature of the rubber is within 80°C, add 0.5 parts of black color masterbatch, catalyst: 2 parts of organotin chelate, crosslinking agent: 4 parts of methyl Tributylketoxime silan...
Embodiment 3
[0040] Select 120 parts of α, ω-dihydroxy polydimethylsiloxane (molecular weight 70000, produced by Shin-Etsu, Japan), and 10 parts of linear polydimethylsiloxane (molecular weight 10000, produced by Dow Corning) whose end group is hydroxyl, after three 15 parts of fumed silica pretreated by functional siloxane and hexamethyldisilazane, 17 parts of aluminum hydroxide pretreated by trifunctional siloxane and D4, 20 parts of melamine cyanurate Mix evenly in the kneader, transfer the rubber material to the three-roll machine for grinding, and then transfer it to the kneader to heat up and stir, keep the temperature of the rubber material at 150°C and the vacuum degree ≥ 0.1Mpa, stir and evacuate Let dry for 4 hours.
[0041] Put the dried rubber into the planetary stirring tank. When the sealing temperature of the rubber is within 100°C, add 1 part of black color masterbatch, catalyst: 3 parts of organotin chelate, crosslinking agent: 5 parts of methyl Tributylketoxime silane, 5...
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