Hierarchical titanium dioxide microspheres based on surface oriented growth nano-rods and preparation method thereof
A titanium dioxide, directional growth technology, applied in the direction of titanium dioxide, chemical instruments and methods, titanium oxide/hydroxide, etc., can solve the problems of unsuitability for large-scale production, low degree of crystallization, poor reproducibility, etc., and achieve good self-settling Performance, good light scattering, excellent performance effects
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Embodiment 1
[0040] A preparation method of graded titanium dioxide microspheres based on surface oriented growth nanorods, comprising the following steps:
[0041] (1) Under the condition of room temperature and constant stirring, the stirring rate is 2000 rpm, and the molar ratio of resorcinol and formaldehyde is 1:8, which are dissolved in water successively, and the amount of water is controlled so that the mass concentration of resorcinol is 1.5%, to get a mixed solution;
[0042] (2) Add titanium trichloride solution dropwise to the resulting mixed solution until the molar ratio of titanium trichloride and resorcinol is 1:8 to obtain a reaction solution; the titanium trichloride solution is dissolved in 3wt % titanium trichloride solution in the hydrochloric acid solution, the concentration of titanium trichloride is 1.5mol / L;
[0043] (3) Transfer the obtained reaction solution into an airtight container, and place it in a constant temperature water bath at 90°C for 2 hours to reac...
Embodiment 2
[0051] A preparation method of graded titanium dioxide microspheres based on surface oriented growth nanorods, comprising the following steps:
[0052] (1) Under the condition of room temperature and constant stirring, the stirring rate is 500 rpm, and resorcinol and formaldehyde are dissolved in water in a molar ratio of 1:2 in sequence, and the amount of water is controlled so that the mass concentration of resorcinol is 3%, to get a mixed solution;
[0053] (2) Add titanium trichloride solution dropwise to the obtained mixed solution until the molar ratio of titanium trichloride and resorcinol is 1:2 to obtain a reaction solution; the titanium trichloride solution is dissolved in 3wt % titanium trichloride solution in hydrochloric acid solution, the concentration of titanium trichloride is 0.1mol / L;
[0054] (3) Transfer the obtained reaction solution into an airtight container, and place it in a constant temperature water bath at 70°C for 4 hours to react to form a dark r...
Embodiment 3
[0057] A preparation method of graded titanium dioxide microspheres based on surface oriented growth nanorods, comprising the following steps:
[0058] (1) Under the condition of room temperature and constant stirring, the stirring rate is 1000 rev / min, and resorcinol and formaldehyde are dissolved in water in a molar ratio of 1:2 in turn, and the amount of water is controlled so that the mass concentration of resorcinol is 3%, to get a mixed solution;
[0059] (2) Add titanium trichloride solution dropwise to the obtained mixed solution until the molar ratio of titanium trichloride and resorcinol is 1:2 to obtain a reaction solution; the titanium trichloride solution is dissolved in 3wt % titanium trichloride solution in hydrochloric acid solution, the concentration of titanium trichloride is 0.5mol / L;
[0060] (3) Transfer the obtained reaction solution into an airtight container, and place it in a constant temperature water bath at 50°C for 6 hours to generate a dark red g...
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