Long-lasting phosphorescent waterborne coating and preparation method thereof

A long-lasting luminescent, water-based coating technology, applied in the direction of luminescent coatings, epoxy resin coatings, polyurea/polyurethane coatings, etc., can solve the problems of only 2 to 3 weeks of application period, easy hydrolysis of photoluminescent materials, etc., and achieve reduction The effect of industrial production cost, easy implementation, and broad application prospects

Inactive Publication Date: 2015-08-26
ZIGONG INNOVATION CENT OF ZHEJIANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The Chinese invention patent application with the publication number CN01122917.9 also discloses a water-based luminescent paint, the technical principle of which mainly uses 20-70 parts by weight of polymer emulsion and 5-60 parts by weight of photoluminescent material, but the paint The photoluminescent material in the product is easy to hydrolyze, and the product's shelf life is only 2 to 3 weeks

Method used

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  • Long-lasting phosphorescent waterborne coating and preparation method thereof
  • Long-lasting phosphorescent waterborne coating and preparation method thereof
  • Long-lasting phosphorescent waterborne coating and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0046] Add 40 parts of absolute ethanol, 60 parts of long afterglow luminous powder (Luming PLO-8C) into the mixer, add 5 parts of silane coupling agent (KH550) dropwise at a speed of 200r / min, and disperse for 10 minutes to obtain a slurry; The slurry was filtered through a 100-mesh sieve, and dried at 80° C. for 2 hours to obtain a hydrophobically modified luminescent powder.

Embodiment 2

[0048] Add 60 parts of absolute ethanol, 40 parts of long afterglow luminescent powder (Luming PLO-8C) into the mixer, add 1 part of titanate coupling agent (AC100) dropwise at a speed of 1000r / min, and disperse for 10 minutes to obtain a slurry material; the slurry was filtered through a 100-mesh sieve, and dried at 80° C. for 2 hours to obtain a hydrophobically modified luminescent powder.

Embodiment 3

[0050] Add 80 parts of absolute ethanol, 20 parts of long afterglow luminescent powder (Luming PLO-8C) into the mixer, add 3 parts of titanate coupling (AC100) dropwise at a speed of 600r / min, and disperse for 10 minutes to obtain a slurry ; The slurry was filtered through a 100-mesh sieve, and dried at 80° C. for 2 hours to obtain a hydrophobically modified luminescent powder.

[0051] In summary, the coating product of this embodiment is prepared from the following raw materials in parts by weight:

[0052] Long afterglow luminescent powder 20-60 parts;

[0053] 40-80 parts of absolute ethanol;

[0054] Hydrophobic modifier 1-5 parts;

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Abstract

The invention relates to functional building coating technologies and aims to provide a long-lasting phosphorescent waterborne coating and a preparation method thereof. The coating is prepared by mixing the following raw materials in parts by weight: 30-50 parts of synthetic resin emulsion, 15-30 parts of hydrophobic modified luminescent powder, 12-30 parts of pigments and fillers, 6.5-8 parts of an assistant and 20-40 parts of de-ionized water. The luminescent powder is subjected to hydrophobic modification to obtain the hydrophobic modified luminescent powder which is stable for a long term (more than 6 months) in a waterborne environment and emits light for 12 hours. The hydrophobic modified luminescent powder is introduced into the coating, so that a film-forming material has the functions of being stable for a long term (more than 6 months) in the waterborne coating and emitting light for 12 hours. At the same time, the preparation method is simple, convenient and favorable for reducing the industrialized production cost. According to the preparation method, the raw materials are ground, stirred and dispersed to prepare the coating; the preparation process is simple, easy to implement, simple and convenient to operate and favorable for large-scale industrialized production, and reduces the industrialized production cost.

Description

technical field [0001] The invention belongs to the technical field of functional architectural coatings, in particular to a long afterglow luminescent water-based coating and a preparation method thereof. Background technique [0002] As an energy storage luminescent material, long afterglow luminescent paint has the advantage of long luminescence time, and its nighttime indicating function is applied in tunnels, signboards, indicator marks and other occasions. However, the luminescent material of the long-lasting luminescent paint is usually an easily hydrolyzed inorganic salt, which usually appears in the form of a solvent-based paint, which pollutes the environment and is not suitable for large-scale use in the construction field. [0003] The Chinese invention patent application with the publication number CN01110277.2 discloses a kind of energy storage luminescent coating, which includes 35-40 parts by weight of modified hydrocarbon volume, 25-35 parts by weight of pol...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D133/04C09D125/14C09D131/04C09D175/04C09D163/00C09D5/22C09D7/12
CPCC09D133/04C08L2205/03C09D5/22C09D7/61C09D7/62C09D7/63C09D125/14C09D175/04C08L1/284C08L91/00C08K13/06C08K9/04C08K3/34C08K5/053C08K5/103C08K5/46C08K2003/2241C08K3/346C08K2003/265C08K9/06
Inventor 杨辉徐意彭晓光姜译翔
Owner ZIGONG INNOVATION CENT OF ZHEJIANG UNIV
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