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616results about How to "Conducive to industrial mass production" patented technology

Epoxy resin composition, preparation method thereof, laminated material and copper-clad laminated board manufactured by adopting epoxy resin composition

The invention relates to an epoxy resin composition, a preparation method thereof, a laminated material and a copper-clad laminated board manufactured by adopting the epoxy resin composition. The epoxy resin composition comprises the following components in part by mass: 30 to 80 parts of epoxy resin, 20 to 50 parts of polyphenyl ether resin with a novel structure, 0 to 50 parts of filler and 1 to 20 parts of assistant, wherein the polyphenyl ether resin is obtained through redistribution reaction of polyphenyl ether and phenolic resin in the presence of a reaction initiator, and the number-average molecular weight of the polyphenyl ether resin is 1,000 to 5,000. The epoxy resin composition provided by the invention not only has good heat resistance and dielectric property, but also has simple and convenient preparation process and is favorable for industrialized large-scale production; and in addition, the laminated material and the copper-clad laminated board manufactured by using the epoxy resin composition are applied to a printed circuit board, have good heat resistance, dielectric property and machining property, and are favorable for signal transmission of a high-frequency circuit board.
Owner:GUANGDONG SHENGYI SCI TECH

Silicon carbon composite material, fabrication method thereof, anode material and battery

The invention relates to a silicon carbon composite material. The silicon carbon composite material comprises a three-layer core-shell structure, wherein a silicon material is arranged at the innermost layer, a metal compound is arranged at the intermediate layer, a carbon material is arranged at the outermost layer, and the silicon material is selected form one or more of silicon, a silicon oxide and a metal silicide. In the above silicon carbon composite material, the intermediate layer of the metal compound is further arranged between the silicon material and the carbon material, the interface contact between the silicon material and the carbon material is effectively improved, so that the silicon carbon composite material is more stable during the application process. The conductivity of the silicon carbon composite material is improved, and the energy density is also improved. The silicon carbon composite material is easier to be bonded with a current collector during the subsequent preparation and application process, and is difficult to be agglomerated or drop, and the cycle performance of the silicon carbon composite material is improved. The fabrication method is low in process difficulty, the device is simple, and the industrial production is facilitated. The invention also discloses a fabrication method of the above silicon carbon composite material, an anode material and a battery.
Owner:SUZHOU GCLSI SCI & TECH IND APPL RES INST CO LTD +3

Polymer based nanocomposite and preparing method thereof

The invention discloses a polymer based nanocomposite and a preparing method thereof. According to the invention, an organic covalent modification technology is adopted, polyhydroxy cyclodextrin molecules are anchored on a graphene oxide nanosheet through a coupling agent, excellent dispersion in various solvents is realized through utilizing the hydroxyl on the cyclodextrin to simulate the characteristic that the graphene oxide is enriched with oxygen species, the capacity of cyclodextrin on the graphene oxide is controlled through adjusting the reaction temperature, further the solvent dispersing performance and thermal stability of functionalized hybrid materials can be effectively regulated and controlled; besides, the solvent blending technology is adopted, the cyclodextrin functionalized grapheme based nano hybrid materials are used as fillers to prepare different-polymer based nanocomposite; through the adoption of the method, the intermolecular and intramolecular interfacial interaction are further enhanced so as to improve the thermal stability of the functionalized nano materials and polymer based nanocomposite adopting the nano materials as fillers, besides, the synthetic steps are simple and efficient, the aftertreatment is simple and concise, and large-scale preparation is facilitated.
Owner:NANJING UNIV OF SCI & TECH

Preparation method of transparent super-hydrophobic zinc oxide coating

The invention relates to a preparation method of a transparent super-hydrophobic zinc oxide coating on a glass substrate. The preparation method comprises the following steps of a, substrate pretreatment; b, zinc oxide solution preparation; c, zinc oxide coating preparation; and d, zinc oxide coating surface modification. Compared with the prior art, the preparation method has the beneficial effects of simple equipment process, low cost and mild reaction condition and is beneficial to large-scale industrial production. The transparent super-hydrophobic zinc oxide coating prepared by using the method has excellent hydrophobicity and transparency; the contact angle is larger than 160 degrees, the rolling angle is smaller than 8 degrees, and water drops can freely roll on the coating, so that the transparent super-hydrophobic zinc oxide coating has relatively good self-cleaning performance; and the light transmittance is approach to 90% which is close to that of blank glass, so that the transparent super-hydrophobic zinc oxide coating has favorable visible light transmittance. A surface modifier used in the preparation method is an alkyl silane coupling agent instead of a fluorinated compound, so that the cost is low, the environment pollution is relatively low, and the modified coating is relatively stable.
Owner:WUHAN INSTITUTE OF TECHNOLOGY

Method for preparing KA oil and derivatives of KA oil by electrocatalytic hydrogenation of lignin-based phenolic compounds

The invention relates to a method for preparing KA oil and derivatives by electrocatalytic hydrogenation of lignin-based phenolic compounds. According to the method, an H-shaped electrolytic cell is used as a container, in a negative pole chamber of the electrolytic cell, carbon fiber cloth is coated with a supported composite catalyst as a working electrode, and the lignin-based phenolic compounds are used as reaction substrates to be dissolved in an acidic solution as a negative pole solution; and a positive pole chamber uses a platinum sheet as a counter electrode and the acidic solution aspositive pole liquid, an electrocatalytic hydrogenation reaction is carried out at the temperature of 30-90 DEG C for 0.5-2 hours, and the KA oil and the derivatives of the KA oil are obtained afterpost-treatment. By the adoption of the method, by adopting the composite catalyst, the service life of the catalyst is greatly prolonged, and the conversion rate of the lignin-based phenolic compoundsreaches over 90-99%, the selectivity of the KA oil and the derivatives of the KA oil reaches over 90-95%, the Faraday efficiency can reach 80-90%, the cost is low, environmental protection is realized, the technological process is simple, the supported composite catalyst is recyclable, the production cost lowered, and the method has the high industrial value.
Owner:ZHEJIANG UNIV OF TECH

Ceramic tile with heating function and preparation method thereof

InactiveCN107097478APrevents heat transfer downwardsImprove heating efficiency and thermal insulation performanceConstructions elementsCeramic layered productsThermal insulationCeramic tiles
The invention discloses a ceramic tile with a heating function. The ceramic tile is prepared by fitting a ceramic tile layer with a ceramic tile base layer with a cavity, wherein the cavity is located on one side of the fitting surface; the cavity is filled with an insulating layer, a heating layer and an insulating sealing heat conducting layer overlapped in turn from bottom to top; a metal electrode and a temperature sensor are arranged in the heating layer. According to the ceramic tile disclosed by the invention, a cavity for filling a heating function composite layer is arranged on one side of the fitting surface between the ceramic tile layer and the ceramic tile base layer, and the layer structure of the composite layer is further limited; by adding a near-infrared inorganic heat reflecting layer, the heat emitted by the heating layer is efficiently transferred to the ceramic tile layer and effectively prevented from being transferred downward, and the heating efficiency and thermal insulation property of the ceramic tile are greatly improved. The invention also discloses a preparation method of the ceramic tile, which has the advantages of simple preparation technology, low production cost and high operability and facilitates industrial large-scale production.
Owner:FOSHAN OCEANO CERAMICS

Beta-FeOOH/polyacrylonitrile composite nanofiber membrane, preparation method thereof and application of membrane

The invention provides a beta-FeOOH / polyacrylonitrile composite nanofiber membrane, a preparation method thereof and an application of the membrane, and belongs to the technical field of materials. The preparation method of the beta-FeOOH / polyacrylonitrile composite nanofiber membrane includes the steps: polyacrylonitrile nanofiber membrane preparation: preparing a polyacrylonitrile nanofiber membrane by electrostatic spinning; stabilizing treatment: performing gradient heating treatment on the polyacrylonitrile nanofiber membrane; biological mineralization treatment: preparing ferric chloridesolution and hydrochloric acid according to the volume ratio of 2:1, placing the stabilized polyacrylonitrile nanofiber membrane into mixed solution and stirring the mixed solution for 1-3 minutes, performing reaction under the condition of 55-65 DEG C for 10-14 hours, and then cleaning and drying the polyacrylonitrile nanofiber membrane to prepare the beta-FeOOH / polyacrylonitrile composite nanofiber membrane. The beta-FeOOH / polyacrylonitrile composite nanofiber membrane has good stability, mechanical performance, super-hydrophilic-underwater super-oleophobic properties and high adsorption efficiency and can be recycled.
Owner:成都石大力盾科技有限公司

Long-lasting phosphorescent waterborne coating and preparation method thereof

The invention relates to functional building coating technologies and aims to provide a long-lasting phosphorescent waterborne coating and a preparation method thereof. The coating is prepared by mixing the following raw materials in parts by weight: 30-50 parts of synthetic resin emulsion, 15-30 parts of hydrophobic modified luminescent powder, 12-30 parts of pigments and fillers, 6.5-8 parts of an assistant and 20-40 parts of de-ionized water. The luminescent powder is subjected to hydrophobic modification to obtain the hydrophobic modified luminescent powder which is stable for a long term (more than 6 months) in a waterborne environment and emits light for 12 hours. The hydrophobic modified luminescent powder is introduced into the coating, so that a film-forming material has the functions of being stable for a long term (more than 6 months) in the waterborne coating and emitting light for 12 hours. At the same time, the preparation method is simple, convenient and favorable for reducing the industrialized production cost. According to the preparation method, the raw materials are ground, stirred and dispersed to prepare the coating; the preparation process is simple, easy to implement, simple and convenient to operate and favorable for large-scale industrialized production, and reduces the industrialized production cost.
Owner:ZIGONG INNOVATION CENT OF ZHEJIANG UNIV

Mn/Co-based low-temperature SCO catalyst and preparation method thereof

The invention discloses a Mn / Co-based low-temperature SOC catalyst and a preparation method thereof. The preparation method comprises the following steps: (1) dissolving manganese-containing metal salt and cobalt-containing metal salt in dimethylformamide, adding an organic ligand and water, and magnetically stirring and uniformly mixing the components to obtain a mixed solution; and (2) carrying out hydrothermal reaction on the obtained mixed solution in a reactor, reacting to obtain Mn / Co double-metal organic framework crystal, soaking the Mn / Co double-metal organic framework crystal in the dimethylformamide and activating the Mn / Co double-metal organic framework crystal, and then purifying, filtering and roasting the activated crystal to obtain the Mn / Co-based low-temperature SCO catalyst. The Mn / Co-based low-temperature SCO catalyst has good low-temperature denitration activity. Compared with an existing low-temperature denitration catalyst, the Mn / Co-based low-temperature SOC catalyst has the advantages that the conversion rate of catalyzed NO is greatly increased, at the low temperature of 150-200 DEG C, the catalyzed conversion rate of NO can reach 50% or above, and existing industrial requirements can be met.
Owner:SOUTH CHINA UNIV OF TECH

Hollow porous spherical mixed oxide for lithium ion battery negative electrode and preparation method of hollow porous spherical mixed oxide

The invention relates to hollow porous spherical mixed oxide for a lithium ion battery negative electrode and a preparation method of the hollow porous spherical mixed oxide. The material is a uniform nano-mixture of Mn2O3 and NiMn2O4, and a specific chemical formula is NixMn<1-x>O<1.5-0.5x> (x is more than 0 and less than 1 / 3). The preparation method of the hollow porous spherical mixed oxide comprises the steps that based on complexing action of ammonia water and nickel ions, the precipitation speed of nickel carbonate is reduced, so that a spherical structure of the manganese carbonate cannot be destroyed by the nickel carbonate and has a certain modification function on a spherical structure of the manganese carbonate to form a uniform spherical mixture (NixMn<1-x>CO3, x is more than 0 and less than 1 / 3) of the nickel carbonate and the manganese carbonate; the prepared hollow porous spherical mixed oxide for the lithium ion battery negative electrode is obtained by using a high-temperature segmental roasting process. Compared with the prior art, the method is easy to operate and suitable for industrial large batch production; by utilizing the hollow porous spherical mixed oxide, the large-current charging / discharging performance of the lithium ion battery negative electrode can be effectively improved, and the and the cycle life of the lithium ion battery negative electrode can be effectively prolonged.
Owner:SHANGHAI JIAO TONG UNIV

Preparation method for non-bonding-phase pure-carbonation tungsten target material

The invention provides a preparation method for a non-bonding-phase pure-carbonation tungsten target material. The method comprises the steps that pure-carbonation tungsten raw material powder is screened firstly to obtain pure-carbonation tungsten powder with the even particle size; then a mould is evenly filled with the pure-carbonation tungsten powder, hot-pressing sintering treatment is conducted under the vacuum condition, cooling is conducted, and then mould release is conducted to obtain a sintered blank; and finally, the sintered blank is machined to obtain the non-bonding-phase pure-carbonation tungsten target material meeting the size and surface-quality requirements. According to the preparation method for the non-bonding-phase pure-carbonation tungsten target material, the technique is simple, the forming effect is good, and industrialized large-scale production is facilitated; the target material does not contain any bonding phase component, grains are even, the average grain size is 5 [mu]m or below, the compactness can reach 99% or more, and the purity is 99.9% or more; and according to the target material, the arc starting discharging phenomenon in the sputtering process is reduced, the surface defects of a prepared film layer are few, a coating is more compact, the target material can be used for preparing an adulteration phase of diamond-like carbon (DLC) coating and a transitional layer, and coating mechanical performance and tribological performance are improved.
Owner:北京安泰六九新材料科技有限公司 +1

Method for preparing light ceramsites by subway rail residue soil

The invention discloses a method for preparing light ceramsites by subway rail residue soil. The method includes the steps: drily grinding the subway rail residue soil by a ball grinder, then sieving the dry grinded residue soil by a sieve with100 meshes, uniformly mixing the sieved residue soil and coal ash according to a weight percentage, and preparing a mixed slurry according to water-solid ratio; performing granulation for the mixed slurry by a granulator to form balls, selecting the balls with grain diameters of 15-25mm and 10-15mm, and placing the selected balls into a constant temperature air blast drying oven with the temperature of 105 DEG C to dry by constant temperature for 4 hours or more than; tiling the dried balls on a ceramic fiber board, placing the tiled balls in a silicon-molybdenum box-type resistance furnace, increasing the temperature to 500 DEG C from the indoor temperature by the heating speed of 8-10 DEG C per minute, preheating for 20 minutes, then increasing the temperature to 1160-1250 DEG C by the heating speed of 8-10 DEG C per minute, roasting for 15 minutes, placing roasted ceramsites in a ventilated kitchen to naturally cool to the indoor temperature, and sieving the roasted ceramsites to obtain the light ceramsites. The weight percentage of the residue soil and the coal ash is 50%-85%:15%-50%, and the water-solid ratio is 15%-30%. The prepared ceramsites meet standard requirements of artificial lightweight aggregates in GB/T17431.1-2010 and GB/T17431.2-2010 and has the excellent advantages of high strength, multiple hole, high temperature resistance and the like and can serve as high-efficiency support agents for precast concrete components and thermal insulation materials of walls.
Owner:TIANJIN CHENGJIAN UNIV

Method for preparing nano MnO2 composite electrode for high-conductivity super-capacitor

A method for preparing nano MnO2 composite electrode for a high-conductivity super-capacitor includes the steps of taking a multi-walled carbon nanotube, adding the multi-walled carbon nanotube to mixed acid formed by sulfuric acid and nitric acid, wherein the molar ratio of the sulfuric acid and the nitric acid is 3:1, heating the mixed acid to 60 DEG C and stirring the mixed acid in a centrifugal mode, washing the mixed acid repeatedly with deionized water until the PH value of supernatant is 7, drying the multi-walled carbon nanotube for use, preparing electrolyte with the concentration between 0.1g / L and 2g / L, using stainless steel net electrodes as a cathode and an anode, applying direct-current voltage of 0.05-1V / cm2 across the cathode and the anode, depositing for 10-50min, obtaining a stainless steel net absorbing the multi-walled carbon nanotube, preparing a MnSO4 solution or a MnNO3 solution of 0.1mol / L as electrolyte, taking the stainless steel net to prepare an electrode, wherein the electrode serves as a positive pole and a platinum electrode serves as a negative pole, carrying out electrodeposition at a constant current of 0.5-50mA / cm2, keeping the temperature at 90 DEG C, and obtaining the nano MnO2 composite electrode after depositing for 5-30min. The method can conveniently and accurately control current density, electrolysis time, the type, components, the concentration, the PH value and other parameters of the electrolyte, and has the advantages of being simple to operate and low in cost.
Owner:NANCHANG HANGKONG UNIVERSITY
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