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36 results about "Tungsten target" patented technology

High-precision wide-energy-spectrum neutron source target body structure

The invention belongs to the technical field of nuclear physics and particle accelerators, and relates to a high-precision wide-energy-spectrum neutron source target body structure applied to a spallation neutron source device. The method comprises the following steps: a tungsten target is adopted, and a 6cm thin target design is adopted; the cooling layer contains boron water and the like and can be used for cooling and slowing down neutrons; the moderation layer moderates the neutron energy spectrum to a thermal neutron energy region by using boron-containing water; the shielding layer is made of low-carbon steel and concrete to ensure radiation safety; the tail end of the neutron channel is connected with an experimental terminal; according to the thin target design, the energy resolution is improved, the energy resolution of neutrons below 100 keV is higher than 0.1%, and the energy resolution of neutrons below 1 MeV reaches 0.3%; the boron element reduces the gamma ray background; and the five neutron pore channels meet various requirements. The overall design realizes the effect required by the high-precision neutron experiment and improves the precision of the device.
Owner:CHINA SPALLATION NEUTRON SOURCE SCI CENT +1

Preparation method of zirconium-coated tungsten target for hash neutron source

The invention provides a preparation method of a zirconium-coated tungsten target for a hash neutron source, and the preparation method comprises the following steps: assembling a first C-shaped zirconium sheet, a second C-shaped zirconium sheet and a tungsten target, and enabling the zirconium sheet to completely coat the tungsten target to obtain an assembly; and the assembly is placed in a sheath, degassing and hot isostatic pressing treatment are conducted in sequence, and the zirconium-coated tungsten target for the hash neutron source is obtained after the sheath is removed. The zirconium-coated tungsten target prepared by the preparation method has the advantages of high mechanical strength, few welding defects and long service life, and can be used as a stable spallation neutron source.
Owner:宁波江丰热等静压技术有限公司

Solidified abrasive particle grinding pad and grinding method for tungsten material

The invention relates to a consolidated abrasive particle grinding pad and a grinding method for tungsten materials, and relates to the technical field of surface machining, the consolidated abrasive particle grinding pad comprises an abrasive particle layer; the abrasive particle layer comprises the following components in percentage by mass: 35-45% of silicon carbide particles, 8-15% of ceramic particles and the balance of resin. According to the fixed abrasive particle grinding pad provided by the invention, through the design of the abrasive particle layer in the grinding pad, when a tungsten material is machined, a good machining effect can be achieved, and the specular reflectance of a tungsten target material obtained after machining is larger than or equal to 92.8% and can reach 96.8% or above in a preferable scheme.
Owner:KONFOONG MATERIALS INTERNATIONAL CO LTD

Sputtering apparatus and method for forming tungsten film

To provide a sputtering system and a film deposition method capable of depositing a low-resistance tungsten film.SOLUTION: The sputtering apparatus includes a substrate stage 2 for holding a substrate Sw in a vacuum chamber 1 in which a target 3 made of tungsten is installed, and a high-frequency power supply Hs for supplying high-frequency power to the substrate stage 2. When a first plasma atmosphere Pm1 is generated in a vacuum chamber 1 and sputtered particles are stuck and deposited on a substrate Sw by sputtering a target 3 to form a tungsten film, high-frequency power is supplied to a substrate stage 2 to generate a second plasma atmosphere Pm2, and positive ions in the first plasma atmosphere Pm1 are also made to collide with the substrate Sw. A ratio of an anode area to a cathode area is set in a range of 4.0 to 6.0, where the cathode area is an area of the substrate holding surface 2a of the substrate stage 2, and the anode area is a surface area in the vacuum chamber 1 functioning as one of the electrodes of the substrate stage 2 and the other of the electrodes of the second plasma atmosphere Pm2.SELECTED DRAWING: Figure 1
Owner:ULVAC INC

Tungsten target composite and method of making same

The application belongs to the technical field of alloy materials, and specifically discloses a tungsten target composite material and a preparation method thereof, which comprises the following steps: (1) adding spherical tungsten powder, spherical titanium powder, sodium carboxymethyl cellulose and polyvinyl alcohol into water, ball-milling and uniformly mixing to obtain a first mixed solution; (2) adding carbon nanotubes and amino silane coupling agent into a nitric acid solution, uniformly stirring to obtain a second mixed solution; (3) uniformly mixing the first mixed solution, flaky molybdenum disulfide powder and the second mixed solution, ultrasonic treatment, and drying to obtain a precursor; and (4) performing degreasing and sintering on the precursor to obtain the tungsten target composite material. The tungsten target composite material has excellent electrical conductivity and mechanical properties, and has a wide application prospect.
Owner:UV TECH MATERIAL CO LTD

A tungsten target and its preparation method

This invention provides a tungsten sputtering target and its preparation method, relating to the field of magnetron sputtering target preparation technology. The preparation method includes first loading tungsten powder into a casing; then performing vacuum hot pressing sintering on the casing filled with tungsten powder. During vacuum hot pressing sintering, the casing isolates the tungsten powder from the carbon atmosphere, preventing the introduction of impurity elements, and simultaneously achieving degassing, sealing, and sintering of the tungsten powder in the casing; followed by hot isostatic pressing. The casing is made of a metal with a melting point higher than 2000℃ that does not chemically react with tungsten. Before vacuum hot pressing sintering, this invention uses a metal casing to fill the tungsten powder, which not only improves the initial density and uniformity of the tungsten powder and increases the contact area between powder particles, thus improving sintering activity; it also prevents carbon elements from intruding into the blank, reducing carbon inclusions, improving the purity of the target material, lowering the sintering temperature and pressure, improving production efficiency, reducing energy consumption, and extending the service life of the mold.
Owner:GRIKIN ADVANCED MATERIALS

Divertor target plate small-angle thermal load simulation device and detection method

The invention discloses a divertor target plate small-angle thermal load simulation device and detection method.The device comprises a discharge unit and an inflation unit arranged at one end of the discharge unit, the discharge unit comprises an insulation block, one end of the insulation block is provided with a first end cover, and the other end of the insulation block is provided with a second end cover; the first end cover, the insulating block and the second end cover are provided with first through holes along the axis, the first through holes are used for installing a copper-tungsten electrode, a first capillary tube, a second capillary tube, a first main electrode and a second main electrode which are connected in sequence, the first capillary tube comprises a first capillary tube accessory and a second capillary tube accessory, and a target groove is formed in the second capillary tube accessory and used for installing a tungsten target; the arrangement of the first gap, the second gap, the third gap and the fourth gap is used for preventing external gas or internal helium plasma from leaking from each connecting part, voltage is applied to the first end cover and the second end cover to break down the gas in the discharge channel, and helium plasma jet is formed under the pushing of pressure and the gas to impact the tungsten target at a small angle.
Owner:XI AN JIAOTONG UNIV

Method for depositing GLC film based on surface of plastic workpiece by adopting PVD (Physical Vapor Deposition) technology

The invention provides a method for depositing a GLC film on the basis of the surface of a plastic workpiece through a PVD technology and the corresponding plastic workpiece. The method comprises the steps that S1, the plastic workpiece is subjected to ultrasonic cleaning and baking; s2, a chromium target, a tungsten target and a graphite target are washed through multi-arc ion plating magnetron sputtering coating equipment; s3, vacuumizing the placed plastic workpiece, and introducing argon to open a chromium target to form a metal chromium layer; s4, starting a chromium target and a tungsten target for introducing argon to form a metal chromium-tungsten layer; s5, argon and nitrogen are introduced for starting a bias power supply, a chromium target and a tungsten target are started, and a chromium tungsten nitride layer is formed; s6, turning on a bias voltage power supply, turning off nitrogen, turning on a chromium target, a tungsten target and a graphite target, and introducing argon and acetylene to adjust bias voltage, so as to form a multi-element nano multilayer film structure; s7, turning on a bias power supply, turning off the tungsten target, turning on the chromium target and the graphite target, and introducing argon and acetylene to form a GLC film layer; and S8, a target material power supply, acetylene, argon and a bias power supply are turned off, and the plastic workpiece is cooled.
Owner:HENGJI COATING (SHENZHEN) CO LTD

Method for preparing and recycling high-purity tungsten target material

The invention belongs to the technical field of magnetron sputtering target material manufacturing, and discloses a method for preparing and recycling a high-purity tungsten target material. According to the preparation and recovery method, used tungsten residual targets serve as raw materials, primary tungsten powder is obtained after mechanical crushing and ball milling, after crushing and ball milling, the primary tungsten powder reacts with fluorine gas at the high temperature to obtain low-purity tungsten hexafluoride with the purity of 2-4 N, and secondary tungsten powder with the purity larger than or equal to 7 N, the O content smaller than or equal to 300 ppm, impurity elements Fe, Ni, Cr, K and Mo smaller than or equal to 0.01 ppm and the average particle size smaller than or equal to 3 micrometers is obtained in a CVD deposition mode. And high-purity tungsten and tungsten alloy target materials can be prepared again by taking the tungsten powder as a raw material.
Owner:GRIKIN ADVANCED MATERIALS

Method for detecting grain size of tungsten target material

The invention provides a method for detecting the grain size of a tungsten target material. The detection method comprises the following steps: (1) carrying out first grinding and polishing treatment and second grinding and polishing treatment on a to-be-detected area of a tungsten target material to obtain a detected surface; (2) performing circumferential sealing and enclosing treatment on the detection surface to form a sealed detection chamber, then injecting etching liquid into the sealed detection chamber to perform etching treatment, and performing cleaning treatment and drying treatment to obtain a detection sample; the etching liquid comprises nitric acid, hydrofluoric acid and sulfuric acid; and (3) observing the metallographic structure of the detection sample by using a portable microscope. The tungsten target material with a smooth and flat interface can be obtained through simple grinding and polishing treatment, a crystal boundary diagram obtained after etching treatment is clear, and the grain size of the tungsten target can be conveniently detected; according to the detection method, different areas of the target material can be detected for multiple times, the overall uniformity of the target material can be effectively known, and local abnormal products are prevented from flowing into clients.
Owner:KONFOONG MATERIALS INTERNATIONAL CO LTD

Electro accelerator and target cooling device thereof

Provided in the present disclosure are an electro accelerator and a target cooling device thereof. The target cooling device comprises a body housing, a liquid inlet, a liquid outlet, a target material and an isolation sheet, wherein a mounting hole is provided in the middle of the body housing; a liquid-cooling cavity is provided inside the body housing; one end of the liquid-cooling cavity is connected to the liquid inlet, and the other end of the liquid-cooling cavity is connected to the liquid outlet; the target material and the isolation sheet are both arranged in the mounting hole, and the target material is arranged above the isolation sheet; and the liquid-cooling cavity comprises a gap between the target material and the isolation sheet. Provided in the present disclosure is a water-cooling heat dissipation mechanism for a target material, the mechanism improving the heat dissipation efficiency, taking away heat in a timely and effective manner, reducing the temperature of the target material, ensuring the efficiency and quality of X-ray generation, and making an apparatus operate more stably and safely. Furthermore, a tungsten target, a flange, a collimator and the heat dissipation structure are integrated into one device, such that the apparatus can have a simplified structure and is easily mounted.
Owner:SHANGHAI BLESSING THE WORLD TECHNOLOGY CO LTD

X-ray diffraction morphology instrument

PendingCN121499565AMaterial analysis using wave/particle radiationLight beamDiffraction topography
The invention discloses an X-ray diffraction morphology instrument, and relates to the technical field of X-ray diffraction detection.The X-ray diffraction morphology instrument comprises a light source structure, a sample bearing structure and an X-ray detector, the sample bearing structure is used for bearing a sample, the light source structure comprises a light source and a capillary element, a tungsten target is adopted as a target material of the light source, and the capillary element is arranged on the light source; the light source is used for generating divergent X-ray light beams, the capillary element is used for gathering the X-ray light beams generated by the light source into focused light beams or collimated light beams and irradiating the focused light beams or collimated light beams onto a sample, and the X-ray detector is used for collecting diffraction imaging signals generated by the sample. The X-ray diffraction morphology instrument provided by the invention can efficiently test the X-ray diffraction morphology of the crystal.
Owner:SUZHOU LIYING TECH CO LTD

Preparation method of fine-grain high-density high-purity tungsten target material

The invention discloses a preparation method of a fine-grain high-density high-purity tungsten target material, which belongs to the technical field of target material preparation, and comprises the following steps: pressing tungsten powder into a blank; the blank is placed on a hollowed-out supporting plate, the blank is sintered into the tungsten porous part under the hydrogen atmosphere which is continuously supplied in a flowing mode, the blank is located on the upstream side of the supporting plate in the hydrogen supply direction and partially covers the hollowed-out through holes, and upstream hydrogen penetrates through the supporting plate from the uncovered through holes to circulate; sleeved hot isostatic pressing treatment is carried out on the tungsten porous part to obtain the tungsten target material, a sheath is provided with a contact layer making contact with a treated workpiece, and the material of the contact layer contains tantalum. Compared with the prior art, the tungsten target material can be sintered in the hydrogen atmosphere in the sintering process, the oxygen impurity content in the tungsten target material is reduced, and the purity of the tungsten target material is improved.
Owner:SHANDONG GEMEI TUNGSTEN & MOLYBDENUM MATERIAL CO LTD

A high-energy x-ray target

The application discloses a high-energy X-ray target, relates to the technical field of X-ray imaging and detection equipment, and comprises a tungsten target, a water cooling system and a double-layer filter, the front surface of the tungsten target is a receiving surface for receiving an electron beam, the back surface is a emitting surface for emitting an X-ray beam, the water cooling system comprises a cooling water pipe, the cooling water pipe is provided with a heat transfer surface which is attached to the edge of the tungsten target, the heat transfer surface is an arc surface along the length direction of the cooling water pipe and is a plane along the width direction, one end of the cooling water pipe is a cooling water inlet for feeding in cooling water, and the other end is a hot water outlet for discharging hot water, and the double-layer filter is opposite to the emitting surface of the tungsten target. Compared with the prior art, the application has more excellent cooling performance, the double-layer filter is arranged to harden the outgoing X-ray, the average energy is improved, and the X-ray detection precision is increased.
Owner:SICHUAN UNIVERSITY OF SCIENCE AND ENGINEERING

Fine-grain tungsten target material and preparation method thereof

The invention relates to the field of sputtering targets for semiconductor manufacturing, and particularly provides a fine-grain tungsten target and a preparation method thereof.The preparation method comprises the steps that 1, halogenated alkane is pre-activated and then subjected to chemical vapor deposition with hydrogen and tungsten hexafluoride on a substrate, and a carbon-doped tungsten material is formed; and (2) the carbon-doped tungsten material is subjected to annealing treatment at the temperature of 1500-2100 DEG C, and the fine-grain tungsten target material is obtained. The preparation method is simple in process, and the prepared tungsten target material has high purity, high density and an equiaxed fine grain structure.
Owner:XIAMEN TUNGSTEN CO LTD

Compact high-stability ECR (electron cyclotron resonance) deuterium-deuterium neutron source device

The invention discloses a compact high-stability ECR (electron cyclotron resonance) deuterium-deuterium neutron source device, and belongs to the technical field of accelerator neutron sources, the device is composed of an ECR ion source, a vacuum chamber and a target body system, and a vacuum pumping system, a high-voltage feed-in system, a microwave feed-in system, a circulating cooling system, a gas supply system and other multifunctional systems are integrated for cooperative work; the ECR ion source adopts three sets of permanent magnet structures to synergistically generate a uniform 875GS magnetic field, and meanwhile, the newly designed microwave window adopts a micro water channel structure and a tungsten target, so that heat deposited in the microwave window can be greatly reduced on the premise of not influencing microwave feed-in, and the service time of the microwave window is doubled; the target and extraction electrode integrated design is adopted, damage of electrons to peek and other insulating materials is reduced, the service life is prolonged, meanwhile, pure zirconium metal is used as the target material, and the deuterium adsorption capacity under the high-temperature condition is greatly improved. The device has the advantages of small size, long-time stable operation and the like.
Owner:INST OF ENERGY HEFEI COMPREHENSIVE NAT SCI CENT (ANHUI ENERGY LAB)

A titanium alloy surface low-temperature permeation and plating integrated composite hardening insulation treatment method

The present invention provides a low-temperature permeation and plating integrated composite hardening insulation treatment method for titanium alloy surface, comprising the following steps: step 1, pickling and etching; step 2, placing the pickled and dried titanium alloy sample into a permeation and plating integrated composite treatment device, wherein the permeation and plating integrated composite treatment device is equipped with a high-energy pulse plasma power supply and a HIPIMS power supply; step 3, kilovolt bias sputtering, pre-injection of nitrogen ions or oxygen ions; step 4, high-power pulse ion nitriding or oxygenation treatment; step 5, sputtering to generate a TiWN-based primer layer: turning on a titanium target and a tungsten target, the titanium target and the tungsten target are controlled by a DC cathode, and a gradient multi-element TiWN coating is prepared by adjusting the ratio of Ti and W; step 6, sputtering to generate a TiWCN base surface layer. The nitriding or oxygenation strengthening operation of the titanium alloy sample substrate and the deposition of a high-hardness insulating coating are completed in the permeation and plating integrated composite treatment device, which can achieve permeation and plating integrated and efficient treatment. Moreover, the nitriding or oxygenation treatment is carried out at a relatively low temperature, and almost no deformation of the titanium alloy substrate occurs.
Owner:CHINA SHIPBUILDING INDUSTRY CORPORATION NO725 RESEARCH INSTITUTE

Tungsten target and method for manufacturing same

To provide a tungsten target in which provision of pores which may cause generation of particles is suppressed, and the size and distribution profile of the pores can be controlled at high precision, and a method for producing the tungsten target. The tungsten target is formed of a sintered product of a tungsten powder. The target has a relative density of 99% or higher, and the number of pores having a size of 0.01 μm2 or more and less than 0.2 μm2 is 20 or less; the number of pores having a size of 0.2 μm2 or more and less than 1.8 μm2 is 5 or less; and the number of pores having a size of 1.8 μm2 or more is 1 or less, when the target is observed in an observation field of 0.15 mm2.
Owner:ULVAC INC

A diffusion bonding method of a chemical vapor deposition tungsten target

The application discloses a diffusion welding method of a chemical vapor deposition tungsten target material and relates to the technical field of target material welding. The diffusion welding method comprises the following steps: providing two groups of tungsten target material assemblies; processing a sine wave tooth structure along a concentric circle on a tungsten plate welding surface of each group of tungsten target material assemblies; processing a second sine wave tooth structure along a spiral line on a back plate welding surface of each group of tungsten target material assemblies; coating a film on the welding surface of each back plate and each tungsten plate; providing a sheath assembly; placing the two groups of tungsten target material assemblies which are oppositely arranged along the thickness direction in a containing cavity, so that the back plates of the two groups of tungsten target material assemblies abut against each other, and an interval layer is arranged between the two back plates; and sequentially performing the following steps on the sheath assembly: pumping, sealing, and hot isostatic pressing diffusion welding, so as to obtain a tungsten target material. The diffusion welding method can guarantee the bonding strength of the welding interface and reduce the risk of cracking or fragmentation of the chemical vapor deposition tungsten target material in the diffusion welding process.
Owner:海朴精密材料(苏州)有限责任公司

Mirror grinding and polishing machining method for tungsten target and application of mirror grinding and polishing machining method

The invention provides a mirror surface grinding and polishing processing method of a tungsten target material and application of the mirror surface grinding and polishing processing method. The mirror surface grinding and polishing processing method comprises chemical mechanical grinding treatment and chemical mechanical polishing treatment which are carried out in sequence. The tungsten target material with a smooth and flat interface can be obtained through grinding-polishing treatment, the interface roughness is reduced to 0.10 [mu] m or below, a crystal boundary diagram obtained through corrosion is clear, and the grain size of the tungsten target can be conveniently detected.
Owner:KONFOONG MATERIALS INTERNATIONAL CO LTD

High-hardness metal tungsten nanocrystalline film and preparation method thereof

The invention provides a high-hardness metal tungsten nanocrystalline film and a preparation method thereof. The preparation method comprises the following steps: cleaning a substrate; the dried substrate is fixed to the center position of a sample table capable of rotating in a two-dimensional mode and conveyed into a cavity through a sample conveying rod; high-purity argon is introduced into the chamber; meanwhile, applying negative bias voltage to the substrate so as to perform ion cleaning and etching on the surface of the substrate; heating the substrate on the sample table; continuously introducing high-purity argon into the chamber, and keeping the temperature of the substrate constant by adopting a high-purity metal tungsten target; then, applying negative bias voltage to the substrate, and coating the substrate by adopting a high-voltage magnetron sputtering technology to obtain a sample; and after coating is finished, vacuumizing the chamber to high vacuum, turning off a heating power supply in a high vacuum state, and taking out the sample through a sample transfer rod after the sample is cooled to room temperature. The method has the technical effects that the film layer quality is high, the uniformity is good, the film forming speed is high, the damage to the film layer is small, the coating thickness is controllable, and the grain size can be controlled.
Owner:ARMOR ACADEMY OF CHINESE PEOPLES LIBERATION ARMY

Sputtering device and method for forming tungsten film

The invention provides a sputtering device capable of forming a low-resistance tungsten film and a film forming method. The present invention is provided with: a substrate stage (2) for holding a substrate (Sw) in a vacuum chamber (1) in which a tungsten target (3) is provided; and a high-frequency power source (Hs) that applies high-frequency power to the substrate stage (2). When a first plasma atmosphere (Pm1) is generated in a vacuum chamber (1) and a tungsten film is formed by depositing sputtering particles on a substrate (Sw) by sputtering of a target (3), a second plasma atmosphere (P2) is generated by applying high-frequency power to a substrate stage (2), and positive ions in the first plasma atmosphere (Pm1) are also caused to collide with the substrate (Sw). The area of the substrate holding surface (2a) of the substrate stage (2) is set as the cathode area, the surface area in the vacuum chamber (1), which functions as one electrode of the substrate stage (2) and as the other electrode of the second plasma atmosphere (P2), is set as the anode area, and the ratio of the anode area to the cathode area is set to be in the range of 4.0-6.0.
Owner:ULVAC INC

Tungsten target material assembly and preparation method thereof

PendingCN121629340AAnodisationVacuum evaporation coatingTungsten targetPorous oxide
The invention relates to a tungsten target material assembly and a preparation method thereof. The tungsten target material assembly sequentially comprises a tungsten target material, an aluminum middle layer and a back plate from top to bottom. The surface of the aluminum intermediate layer is provided with a porous oxide film. The porous oxidation film is arranged on the surface of the aluminum middle layer, the thickness of an element diffusion layer in tungsten and aluminum and the thickness of an element diffusion layer in aluminum and a back plate can be increased due to the existence of the porous oxidation film, the mechanical interlocking degree between every two adjacent layers is increased, and then the bonding strength of the tungsten target material assembly is improved.
Owner:KONFOONG MATERIALS INTERNATIONAL CO LTD

Methods for producing radionuclides

A method for producing a radionuclide comprises irradiating a target material with a linear accelerator to produce a radionuclide, dissolving the irradiated target material comprising the radionuclide, and separating the radionuclide from the irradiated target material. The irradiated target material may be dissolved in an acidic solution comprising one or more mineral acids. The target material may include a tungsten target material, such as a natural tungsten target material comprising one or more of 180W, 182W, 183W, 184W, and 186W or a tungsten target material exhibiting an elemental purity of about 99.95%. Additional methods for producing tantalum radioactive isotopes are disclosed.
Owner:BATTELLE ENERGY ALLIANCE LLC

Large-size crack-free fine-grained high-purity tungsten sputtering target and method for manufacturing the same

PendingCN122352897ACrack freeGlycerol
The embodiment of the application discloses large-size crack-free fine-grain high-purity tungsten sputtering target material and a preparation method thereof; the method comprises the following steps: S1, selecting high-purity tungsten powder raw material; the particle size range of the tungsten powder raw material is 0.47-1.89 mu m, D10=0.47 mu m, D50=1.07 mu m, D90=1.89 mu m, and Span=1.32; S2, the selected high-purity tungsten powder raw material is pretreated by using a glycerol-ethanol mixed solution, and dried to obtain pretreated tungsten powder; S3, the pretreated tungsten powder is cold isostatic pressing forming to obtain a tungsten green body; S4, the tungsten green body is vacuum pre-sintering to obtain a vacuum pre-sintering compact; S5, the vacuum pre-sintering compact is sealed in a niobium-based sheath to obtain a sealed compact body; S6, the sealed compact body is hot isostatic pressing sintering to obtain a tungsten target compact body; and S7, the tungsten target compact body is machined to obtain the large-size crack-free fine-grain high-purity tungsten sputtering target material.
Owner:ZHENGZHOU UNIV +1

Preparation method of fine-grain high-density high-purity tungsten target material

The application discloses a preparation method of fine-grain high-density high-purity tungsten target material and belongs to the technical field of target material preparation. The method comprises the following steps: tungsten powder is pressed into a blank; the blank is placed on a hollow supporting plate, and the blank is sintered into a tungsten porous piece under a continuously flowing hydrogen atmosphere; the blank is located on the upstream side of the supporting plate along the hydrogen supply direction and partially covers the hollow perforations; upstream hydrogen penetrates the supporting plate through the uncovered perforations; a tungsten target material is obtained by performing a hot isostatic pressing treatment on the tungsten porous piece; a sleeve is provided with a contact layer in contact with the treated workpiece, and the contact layer is made of tantalum. Compared with the prior art, the application can sinter the tungsten target material in a hydrogen atmosphere during the sintering process, reduces the oxygen impurity content in the tungsten target material, and improves the purity of the tungsten target material.
Owner:SHANDONG GEMEI TUNGSTEN & MOLYBDENUM MATERIAL CO LTD

Method for manufacturing hard mask

The invention provides a method for manufacturing a hard mask, wherein a tungsten film is used as a fine crystal film, and the film stress can be adjusted according to the film thickness. The method includes: a first step of forming a tungsten nitride film (Ly1) on the surface of a substrate (Sw) to be processed by a reactive sputtering method by introducing a rare gas and a nitrogen gas into a processing chamber of a vacuum atmosphere with a tungsten target as a target; and a second step in which a tungsten film Ly2 is formed on the surface of the tungsten nitride film by a sputtering method in a processing chamber in a vacuum atmosphere, with a tungsten target as a target. In the first step, the flow rate ratio of the rare gas to the nitrogen gas is set to 1.5 or less and the pressure in the processing chamber is set to 1 Pa or more, and in the second step, the stress corresponding to the film thickness of the tungsten film is adjusted by controlling at least one of the total pressure in the processing chamber and the bias power applied to the substrate to be processed at the time of film formation.
Owner:ULVAC INC

A method for preparing a tungsten target material

This invention relates to the field of refractory metal sputtering targets for semiconductor integrated circuits. Specifically, it relates to a method for preparing a tungsten sputtering target and the tungsten sputtering target prepared by this method. This invention uses a molding process to prepare a tungsten blank, which helps reduce waste caused by blank shaping and reduces workload. A vacuum pre-sintering process is then performed to obtain a tungsten blank with a certain strength, while simultaneously reducing the gas content of the sintered blank. Next, the pre-sintered tungsten blank is wrapped with tungsten foil, sealed in a sleeve, and then buried in sand for hot isostatic pressing (HIP) densification. During HIP, the sleeve material melts and mixes with the sand, reducing contamination of the tungsten blank by the sleeve at high temperatures. The dense tungsten foil layer protects the internal high-purity tungsten blank. Finally, machining yields a high-purity, fine-grained, and high-density tungsten sputtering target. This invention's preparation method helps solve the contradiction between density and grain size in tungsten sputtering targets, reduces the gas content of the tungsten sputtering target, and minimizes impurity contamination.
Owner:ADVANCED TECHNOLOGY & MATERIALS CO LTD

Preparation method of tungsten oxide-based memristor and target tracking system

The present application relates to a tungsten oxide-based memristor preparation method and a target tracking system, wherein the tungsten oxide-based memristor preparation method comprises the following steps: cleaning indium tin oxide glass for a set time to obtain a bottom electrode; growing a tungsten target on the bottom electrode by direct current magnetron sputtering to obtain a tungsten oxide film and form a first resistance change layer; growing an indium gallium zinc oxide target on the first resistance change layer by radio frequency magnetron sputtering to obtain an indium gallium zinc oxide film and form a second resistance change layer; and obtaining a silver top electrode by covering a mask plate and direct current magnetron sputtering to form a top electrode. The performance of the memristor is stable, the preparation process is simple, the repeatability is high, the thin film uniformity is good, the multi-level resistance state regulation and the modulation of the memristor behavior can be easily realized by changing the preparation parameters and the test parameters, the target tracking system based on the memristor can realize the brain synapse bionic function, and can be widely applied to simulate the human brain to realize higher-level cognitive functions.
Owner:UNIV OF JINAN

Target assembly and method for manufacturing same

The invention provides a target assembly and a method for manufacturing the target assembly, and the target assembly can suppress the formation of intermetallic compound layers between an aluminum or aluminum alloy plate insertion material and a copper alloy back plate and between a tungsten target material and the insertion material, thereby preventing the reduction of bonding strength. Specifically, the present invention provides a target assembly obtained by sandwiching an aluminum or aluminum alloy plate insertion material between a target material containing tungsten or molybdenum and a copper or copper alloy backing plate and performing diffusion bonding, the target material and the insertion material and the back plate and the insertion material are diffusion bonded via a metal thin film layer, and the metal thin film layer contains Ti, V, Cr, Nb, Pd, Ir, Pt and an alloy containing at least one of these metals, and has a thickness of more than 0.1 [mu] m and 3.0 [mu] m or less.
Owner:ULVAC INC