A kind of multiple free radical synergistic water treatment method under plasma environment
A synergistic, water treatment technology, applied in the field of water pollution prevention and control, can solve problems such as application limitation and narrow pH range, and achieve the effects of wide application range, good repeatability, and novel and reasonable design.
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Embodiment 1
[0058] (1) First draw the standard curve of the organic dye RhB, take different concentrations of the aqueous solution of the organic dye RhB, measure the fluorescence intensity, and draw the standard curve.
[0059] (2) Preparation of active nanoparticles with Au@SiO2 core-shell structure, the preparation steps are as follows: First, take a three-necked flask and add 100mL of distilled water, 40mL of ethanol, and 0.640g of CTAB solid powder in a 70°C water bath at 600r / h The reaction was stirred at min speed for 10 minutes, and the HAuCl 4 ·3H 2 O (55g / 5mL water) was injected into the solution to react for 5min, then 200uL (2M) NaOH was added to generate the nuclei of nanoparticles instantaneously, and the reaction was stirred for 30min for nucleation and growth. Next, 1 mL of TEOS was added dropwise to the solution. Another 400 uL of NaOH (2M) was added to initiate co-polymerization. After 1.5 min, a thin purple coating of gold nanoparticles can be observed. The sol-gel ...
Embodiment 2
[0064] (1) Draw the standard curve of the organic dye EY first, take the aqueous solution of the organic dye EY with different concentrations, measure its fluorescence intensity, and draw the standard curve. (2) Au@SiO 2 The preparation of active nanoparticles with a core-shell structure, the preparation steps are as follows: First, take a three-neck flask and add 100mL of distilled water, 40mL of ethanol, and 0.640g of CTAB solid powder in turn, and stir the reaction at 600r / min in a water bath at 70°C for 10 minutes, the HAuCl 4 ·3H 2 O (55g / 5mL water) was injected into the solution to react for 5min, then 200uL (2M) NaOH was added to generate the nuclei of nanoparticles instantaneously, and the reaction was stirred for 30min for nucleation and growth. Next, 1 mL of TEOS was added dropwise to the solution. Another 400 uL of NaOH (2M) was added to initiate co-polymerization. After 1.5 min, a thin purple coating of gold nanoparticles can be observed. The sol-gel reaction ...
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