Viscosity breaker and production technique thereof
A production process and technology of viscosity reducer, applied in the field of viscosity reducer and its production process, can solve the problems that the viscosity reducer does not have temperature resistance, is not allowed to be used in large quantities, and the viscosity reducer loses its effectiveness, and achieves automation. The effect of continuous production, improved utilization rate and low cost
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Embodiment 1
[0040] A kind of production technology of viscosity reducing agent, carries out successively according to following steps:
[0041] 1) Dissolving 3 parts by mass of 3-glycidylpropyltrimethoxysilane in 4 parts by mass of propanol;
[0042] 2) Separate sepiolite, octyl epoxy stearate, sodium polyacrylate, sodium hydroxide, 3-glycidylpropyltrimethoxysilane dissolved in propanol, and water to 32 parts by mass, Put 21 parts, 9 parts, 7 parts, 7 parts, and 24 parts into the preset reaction kettle, evacuate to make the vacuum degree 5Pa, raise the temperature, and keep the vacuum degree at 10Pa;
[0043] 3) After 5 hours, stop vacuuming, fill the preset reactor with nitrogen, and keep the nitrogen pressure in the preset reactor at 90kPa;
[0044] 4) After 3 hours, stop filling the nitrogen gas and cool down to normal temperature to obtain the liquid product.
Embodiment 2
[0046] A kind of production technology of viscosity reducing agent, carries out successively according to following steps:
[0047] 1) Dissolving 4 parts by mass of N-(β-aminoethyl)-α-aminopropyltrimethoxysilane in 5 parts by mass of propanol;
[0048] 2) Separate sepiolite, octyl epoxy stearate, sodium polyacrylate, sodium hydroxide, 3-glycidylpropyltrimethoxysilane dissolved in propanol, and water to 38 parts by mass, Put 23 parts, 13 parts, 9 parts, 9 parts, and 8 parts into the preset reaction kettle, vacuumize to make the vacuum degree 20Pa, raise the temperature, and keep the vacuum degree at 50Pa;
[0049] 3) After 6 hours, stop vacuuming, fill the preset reactor with nitrogen, and keep the nitrogen pressure in the preset reactor at 95kPa;
[0050] 4) After 4 hours, stop filling the nitrogen gas and cool down to normal temperature to obtain the liquid product.
Embodiment 3
[0052] A kind of production technology of viscosity reducing agent, carries out successively according to following steps:
[0053] 1) Dissolving 5 parts by mass of N-(β-aminoethyl)-α-aminopropyltrimethoxysilane in 6 parts by mass of propanol;
[0054] 2) Separate sepiolite, octyl epoxy stearate, sodium polyacrylate, sodium hydroxide, 3-glycidylpropyltrimethoxysilane dissolved in propanol, and water to 40 parts by mass, Put 24 parts, 14 parts, 10 parts, 11 parts, and 1 part into the preset reaction kettle, vacuumize to make the vacuum degree 35Pa, raise the temperature, and keep the vacuum degree at 100Pa;
[0055] 3) After 7 hours, stop vacuuming, fill the preset reactor with nitrogen, and keep the nitrogen pressure in the preset reactor at 100kPa;
[0056]4) After 5 hours, stop filling the nitrogen gas and cool down to normal temperature to obtain the liquid product.
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