Dibutyl itaconate modified acrylic resin and preparation method thereof
A technology of dibutyl itaconate and acrylic resin, which is applied in the field of paint, can solve the problems of paint viscosity, high paint cost, and the molecular weight of the plasticizer is not too large, so as to achieve good wettability and improve the overall performance
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Embodiment 1
[0009] Dibutyl itaconate modified acrylic resin, its components by mass parts are as follows: xylene 30g, butyl acetate 10g, acrylic acid 3g, styrene 21g, methyl methacrylate 12g, butyl acrylate 20g, clothing Dibutyl conate 2g, acrylamide 1g, di-tert-butyl peroxide 1g.
[0010] Its preparation method is: add xylene and butyl acetate into the reaction kettle according to the formula amount, gradually raise the temperature to the reflux temperature (130°C), and then add acrylic acid, styrene, methyl methacrylate, butyl acrylate, itaconic Acrylic acid dibutyl ester, acrylamide, and di-tert-butyl peroxide were weighed and added to the dripping kettle in sequence. After the temperature in the reaction kettle reached reflux, di-tert-butyl peroxide was also added to the dripping kettle and Stir for 15-20 minutes until evenly mixed, then add the materials in the dripping kettle dropwise to the reaction kettle for 4-5 hours. Sampling, testing, packaging.
Embodiment 2
[0012] The components are as follows in parts by mass: 20 g xylene, 15 g butyl acetate, 8 g acrylic acid, 15 g styrene, 15 g methyl methacrylate, 17 g butyl acrylate, 5 g dibutyl itaconate, 3 g acrylamide, Di-tert-butyl oxide 2g.
[0013] Its preparation method is with embodiment 1.
Embodiment 3
[0015] Dibutyl itaconate modified acrylic resin, its percentage by mass parts is as follows, xylene 34g, butyl acetate 5g, acrylic acid 5g, styrene 25g, methyl methacrylate 10g, butyl acrylate 15g, itaconic Acrylic acid dibutyl ester 3g, acrylamide 2g, di-tert-butyl peroxide 1g.
[0016] Its preparation method is with embodiment 1.
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