Shell powder, preparation method thereof, modification method thereof and application thereof
A technology of shell powder and shell powder, applied in the direction of botanical equipment and methods, applications, chemicals for biological control, etc.
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preparation example 0
[0102] Preparation Example 0: Preparation of Shell Powder
[0103] (1) The washed shells are sequentially calcined in a three-stage gradient, and the specific calcination operation is as follows:
[0104] A1: Calcining at 400°C for 12 minutes;
[0105] A2: Raise the temperature to 500°C at a heating rate of 10°C / min, and keep the temperature for calcination for 22 minutes;
[0106] A3: Raise the temperature to 700°C at a heating rate of 5°C / min, and keep it for calcination at this temperature for 35 minutes. After the calcination is completed, cool it down to room temperature naturally to obtain the calcined shell;
[0107] (2) Pulverize and grind the calcined shells, and pass through a 300-mesh sieve to obtain the shell powder, which is named as BKF.
preparation example 1
[0108] Preparation Example 1: Preparation of Modified Shell Powder
[0109] B1: Obtain shell powder BKF according to the same method as above-mentioned preparation example 0, namely implement the following steps:
[0110] (1) The washed shells are sequentially calcined in a three-stage gradient, and the specific calcination operation is as follows:
[0111] A1: Calcining at 400°C for 12 minutes;
[0112] A2: Raise the temperature to 500°C at a heating rate of 10°C / min, and keep the temperature for calcination for 22 minutes;
[0113] A3: Raise the temperature to 700°C at a heating rate of 5°C / min, and keep it for calcination at this temperature for 35 minutes. After the calcination is completed, cool it down to room temperature naturally to obtain the calcined shell;
[0114] (2) crushing and grinding the calcined shells, and passing through a 300-mesh sieve to obtain the shell powder;
[0115] B2: Add diethanolamine and absolute ethanol to n-butyl titanate (wherein the mol...
preparation example 11-17
[0117] Preparation Example 1.1-1.7: Preparation of Modified Shell Powder
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