Nicotine adsorbent and preparation method thereof
An adsorbent and nicotine technology, applied in chemical instruments and methods, other chemical processes, inorganic chemistry, etc., can solve problems such as death and cigarette pollution, and achieve high adsorption rate, low production cost, and strong nicotine capacity.
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Embodiment 1
[0022] The preparation method of nicotine adsorbent is characterized in that comprising the following steps:
[0023] (1) Preparation of raw mordenite powder: by mole fraction, SiO 2 for 12 parts, Al 2 o 3 is 1 part, NaOH is 2.4 parts, H 2 O is 12 parts; put the above raw materials into the reaction kettle and stir to form a colloid, then continue to stir and age at room temperature for 4 hours, and then crystallize and react at 180°C for 10 hours to obtain the reaction product; Washing with water until the pH value is neutral, then suction filtering to obtain a solid product, and drying the solid product in an oven at 120° C. for 9 hours at a constant temperature to obtain the original powder of mordenite;
[0024] (2) Mixing of powder materials: Put the raw mordenite powder and attapulgite powder prepared in step (1) into the mixer evenly in a weight ratio of 4:1, and stir and mix in the mixing mixer for 1.5 hours;
[0025] (3) Forming and granulation: Put several seeds ...
Embodiment 2
[0033] The preparation method of nicotine adsorbent is characterized in that comprising the following steps:
[0034] (1) Preparation of raw mordenite powder: by mole fraction, SiO 2 for 15 parts, Al 2 o 3 is 1 part, NaOH is 9 parts, H 2 O is 90 parts; put the above-mentioned raw materials into the reactor and stir and mix them into a colloid, then continue to stir and age at room temperature for 6 hours, and then crystallize and react at 170°C for 18 hours to obtain the reaction product; washing with water until the pH value is neutral, and then suction filtering to obtain a solid product, which is dried in an oven at 120°C for 10 hours at a constant temperature to obtain the original powder of mordenite;
[0035] (2) Mixing of powder materials: Put the raw mordenite powder and attapulgite powder prepared in step (1) into the mixer evenly in a weight ratio of 4:1.5, and stir and mix in the mixing mixer for 2 hours;
[0036] (3) Forming and granulation: Put several seeds i...
Embodiment 3
[0043] The preparation method of nicotine adsorbent is characterized in that comprising the following steps:
[0044] (1) Preparation of mordenite raw powder: SiO 2 、Al 2 o 3 , NaOH, H 2 O is the raw material, in parts by mole, SiO 2 for 18 parts, Al 2 o 3 is 1 part, NaOH is 18 parts, H 2 O is 225 parts; put the above raw materials into the reactor and stir to form a colloid, then continue to stir and age at room temperature for 6 hours, and then crystallize and react at 170°C for 18 hours to obtain the reaction product; washing with water until the pH value is neutral, and then suction filtering to obtain a solid product, which is placed in an oven at 120°C and dried at a constant temperature for 11 hours to obtain the original powder of mordenite;
[0045] (2) Mixing of powder materials: put the raw mordenite powder and attapulgite powder prepared in step (1) into the mixer evenly in a weight ratio of 4:1.5, and stir and mix in the mixing mixer for 2.5 hours;
[0046...
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