High-storability release agent and preparation method thereof
A release agent and storage-resistant technology, used in manufacturing tools, casting and molding equipment, metal processing equipment, etc., can solve the problems that the release agent is not easy to store for a long time, the viscosity of the release agent increases, and the release agent is difficult to bond.
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[0017] The present invention also provides a preparation method of a storage-resistant release agent, comprising:
[0018] 1) Soak the vermiculite in a hydrochloric acid solution after calcining, and then filter to obtain the modified vermiculite;
[0019] 2) Mixing modified vermiculite, sodium alginate, soybean wax, dibutyltin dilaurate, nonylphenol ether polyoxyethylene ether, aluminum oxide and an organic solvent to prepare a release agent.
[0020] In the above-mentioned preparation method, the specific type of organic solvent can be selected in a wide range, as long as other components can be uniformly dispersed in the organic solvent, but in order to make the prepared mold release agent have more excellent Viscosity and anti-settling properties, preferably, the organic solvent is selected from one or more of ethyl acetate, ethanol and n-hexane.
[0021] In the above-mentioned preparation method, the specific content of each component can be selected in a wide range, but...
Embodiment 1
[0028] 1) Calcining the vermiculite at 600° C. for 12 hours, soaking it in a hydrochloric acid solution (the concentration of hydrochloric acid is 25% by weight) at 40° C. for 7 hours, and then filtering to obtain the modified vermiculite;
[0029] 2) Mix modified vermiculite, sodium alginate, soybean wax, dibutyltin dilaurate, nonylphenol ether polyoxyethylene ether, aluminum oxide and organic solvent (weight ratio is 85:25:4:4:5:27 : 100) were mixed at 25°C for 45 minutes to prepare the release agent A1.
Embodiment 2
[0031] 1) Calcining the vermiculite at 550° C. for 10 h, soaking it in a hydrochloric acid solution (the concentration of hydrochloric acid is 20% by weight) at 35° C. for 6 h, and then filtering to obtain the modified vermiculite;
[0032] 2) Mix modified vermiculite, sodium alginate, soybean wax, dibutyltin dilaurate, nonylphenol ether polyoxyethylene ether, aluminum oxide and organic solvent (the weight ratio is 75:10:3:2:2:25 : 100) mixed at 15°C for 30 minutes to prepare release agent A2.
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