Preparation method of beta-cyclodextrin modified macroporous amino glucan adsorbent
A technology of aminodextran and pore amino group is applied in the field of preparation of biological adsorbents to achieve the effects of good adsorption selection, large adsorption capacity and fast adsorption speed.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0024] (1) Water phase A: In the reactor, prepare an aqueous solution with a mass percentage of 45% aminodextran to obtain water phase A;
[0025] (2) Organic phase B: In the reactor, add ethyl acetate: 86 mL, bisphenol A diglycidyl ether: 15 g, and Span 80: 8 g, stir and uniformly to obtain organic phase B;
[0026] (3) Preparation of macroporous aminodextran gel: in the reactor, add organic phase B: 60mL, the temperature rises to 65±3℃ constant temperature, stir, add water phase A: 32mL, stir evenly, add 50% by mass NaOH: 8mL, stirred and refluxed for 3.5h, washed thoroughly with distilled water until neutral, filtered, placed in a plastic container and placed in a freeze-drying box, freeze-dried for 24h, ground and sieved to obtain Macroporous aminodextran gel;
[0027] (4) Preparation of β-cyclodextrin modified macroporous aminodextrin adsorbent: In the reactor, add separately, N,N-dimethylformamide: 58mL, β-cyclodextrin: 14g, stir to dissolve Then, add macroporous aminodextran...
Embodiment 2
[0029] (1) Water phase A: In the reactor, prepare an aqueous solution with a mass percentage of 40% aminodextran to obtain water phase A;
[0030] (2) Organic phase B: In the reactor, add ethyl acetate: 89mL, bisphenol A diglycidyl ether: 10g, and Span 80: 10g, stir and uniformly, to obtain organic phase B;
[0031] (3) Preparation of macroporous aminodextran gel: in the reactor, add organic phase B: 65mL, the temperature rises to 65±3℃ constant temperature, stir, add water phase A: 30mL, stir evenly, add 50% by mass NaOH: 5mL, stir and reflux for 3h, wash thoroughly with distilled water to neutrality, filter, place in a plastic container and put in a freeze-drying box, freeze-dry for 24h, grind and sieve to obtain Pore aminodextran gel;
[0032] (4) Preparation of β-cyclodextrin modified macroporous aminodextran adsorbent: In the reactor, add N,N-dimethylformamide: 63mL, β-cyclodextrin: 10g, stir to dissolve Then, add macroporous aminodextran gel: 22g, warm to 55±2℃ constant tem...
Embodiment 3
[0034] (1) Water phase A: In the reactor, prepare an aqueous solution with a mass percentage of 50% aminodextran to obtain water phase A;
[0035] (2) Organic phase B: In the reactor, add ethyl acetate: 84 mL, bisphenol A diglycidyl ether: 20 g, and Span 80: 5 g, stir and uniformly to obtain organic phase B;
[0036] (3) Preparation of macroporous aminodextran gel: In the reactor, add the organic phase B: 55mL, the temperature rises to 65±3℃ constant temperature, stir, add the water phase A: 38mL, stir evenly, add NaOH with a mass percentage concentration of 50%: 7mL, stir and reflux for 4h, wash thoroughly with distilled water to neutrality, filter, put it in a plastic container and put it in a freeze-drying box, freeze-dry for 24h, grind and sieve to obtain Pore aminodextran gel;
[0037] (4) Preparation of β-cyclodextrin modified macroporous aminodextran adsorbent: In the reactor, respectively add, N,N-dimethylformamide: 53mL, β-cyclodextrin: 18g, stir to dissolve Then, add ma...
PUM
Property | Measurement | Unit |
---|---|---|
adsorption capacity | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com