The application discloses a preparation method of an antibiotic selective adsorbent, first, C-BN
nanosheet balls are prepared by a simple catalytic thermal
evaporation method; second, the C-BN
nanosheet balls are used as a main body to limit and load magnetic Fe3O4 nanoparticles; and then mesoporous SiO2 and imprinted polymers are coated on the surface of the C-BN
nanosheet balls in sequence, and the
tetracycline antibiotic selective adsorbent is obtained after template molecules are eluted. The
tetracycline antibiotic selective composite adsorbent with high adsorption capacity is prepared, the high specific surface area of the
carrier material and the enrichment antibiotic capacity of the radial structure and the selectivity of the surface
molecular imprinting material are fully utilized, the
selective adsorption of specific
antibiotics in a complex solution is effectively realized, and the adsorption efficiency is effectively improved. The carbon-doped BN and the limited loading magnetic particles enhance the adsorption capacity, and the adsorbent can be quickly recovered and separated under an external
magnetic field. Meanwhile, the SiO2 layer and the imprinted polymers enable the
antibiotics to be quickly desorbed, and the cycle number is more, so that the antibiotic selective adsorbent has application prospects in the fields of
sewage treatment and food antibiotic detection.