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Preparation method for aluminum alloy semi-solid slurry induced and impregnated by modificator

A semi-solid slurry and aluminum alloy technology, which is applied in the field of metal material preparation, can solve the problems of large equipment investment, stirring dead zone, serious magnetic leakage, etc., and achieve the effects of no three-waste pollution, uniform distribution and fine grain size.

Active Publication Date: 2016-01-13
江西剑发铝型材有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, the mechanical stirring method has the following disadvantages: the molten metal is easily polluted and corroded by the stirrer, and it is easy to be involved in gas and inclusions after a long time, and there is a stirring dead zone, which affects the quality of the semi-solid billet
The isothermal heat treatment method has the following disadvantages: the process parameters such as heating temperature and holding time are difficult to control
Among them, the electromagnetic stirring method has the following disadvantages: the investment in equipment is large, the electromagnetic gap of the device is large, the magnetic flux leakage is serious, and a large part of the energy cannot be used for stirring the metal melt, which greatly increases the production cost.
The near-liquidus method has the following disadvantages: the preparation cycle is long, and it is difficult to accurately control the pouring temperature of the melt

Method used

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  • Preparation method for aluminum alloy semi-solid slurry induced and impregnated by modificator

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Put the Al-Si-Cu alloy ingot into a graphite crucible and overheat it to 740 °C to completely melt the aluminum block, then refine and remove slag, and then add a small piece of Al-9Sr master alloy (the mass fraction of Sr is 9wt.%), Prepare the aluminum alloy whose mass fraction of Sr in the melt is 0.01wt.%, then raise the temperature of the furnace to 760°C and keep it warm for 15 minutes, then place the preheated ultrasonic horn probe in the melt, and apply Intermittent ultrasound, the interval between each ultrasound is 1s, the release time of each ultrasound is 2.0s, the ultrasound power is 1.0kw, the ultrasound frequency is 20kHz, the total ultrasound time is 3min, after the ultrasound is finished, it is cooled to 610°C with the furnace and left standing Keep warm for 8 minutes, and then apply intermittent ultrasound to the melt again. The interval between each ultrasound is 1s, the release time of each ultrasound is 2.0s, the ultrasound power is 1.0kw, the ultras...

Embodiment 2

[0019] Put the Al-Si-Cu alloy ingot into a graphite crucible and overheat it to 745°C to completely melt the aluminum block, then refine and remove slag, and then add a small piece of Al-Sr master alloy (the mass fraction of Sr is 10wt.%), Formulate an aluminum alloy with a mass fraction of Sr in the melt of 0.05wt.%, then heat it up to 765°C with the furnace and keep it warm for 18 minutes, then place the preheated ultrasonic horn probe in the melt, and apply Intermittent ultrasound, the interval between each ultrasound is 2s, the release time of each ultrasound is 2.0s, the ultrasound power is 1.5kw, the ultrasound frequency is 20kHz, the total ultrasound time is 4min, after the ultrasound is finished, it is cooled to 595°C with the furnace and left standing Keep warm for 9 minutes, then apply intermittent ultrasound to the melt again, the interval between each ultrasound is 2s, the release time of each ultrasound is 2.0s, the ultrasonic power is 1.5kw, the ultrasonic frequen...

Embodiment 3

[0021] Put the Al-Si-Cu alloy ingot into a graphite crucible and superheat it to 750 °C to completely melt the aluminum block, then refine and remove slag, and then add a small piece of Al-Sr master alloy (the mass fraction of Sr is 11wt.%), Formulate an aluminum alloy with a mass fraction of Sr in the melt of 0.09wt.%, then heat it up to 770°C with the furnace and keep it warm for 20 minutes, then place the preheated ultrasonic horn probe in the melt, and apply Intermittent ultrasound, the interval between each ultrasound is 2s, the release time of each ultrasound is 2.5s, the ultrasound power is 2.0kw, the ultrasound frequency is 20kHz, the total ultrasound time is 5min, after the ultrasound is finished, it is cooled to 585°C with the furnace and left standing Keep warm for 10 minutes, then apply intermittent ultrasound to the melt again, the interval between each ultrasound is 2s, the release time of each ultrasound is 2.5s, the ultrasonic power is 2.0kw, the ultrasonic freq...

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Abstract

A preparation method for aluminum alloy semi-solid slurry induced and impregnated by a modificator comprises the following steps that (1) an Al-Si-Cu alloy ingot is placed into a graphite crucible to be subjected to fusion, refining and slag removal; (2) small pieces of Al-Sr intermediate alloy are added into the fondant, the mass fraction of Sr in the Al-Sr intermediate alloy is 9 wt.%-11 wt.%, and the mass fraction of the Sr in the fondant is 0.01 wt.%-0.09 wt.%; (3) the temperature is increased to 760-770 DEG C, heat preservation is conducted for 15-20 min, then a preheated ultrasonic amplitude-change pole probe is placed in the fondant, ultrasounds are released intermittently, the ultrasound interval of each time is 1-2 s, the ultrasounds are released for 2.0-2.5 s each time, the power is 1.0-2.0 kw, the frequency is 20 kHz, the total ultrasound time is 3-5 min, then the temperature is decreased to 585-610 DEG C, and standing and heat preservation are conducted for 8-10 min; and (4) intermittent ultrasound treatment is conducted on the fondant again, the ultrasound conditions are identical to those in the step (3), the total ultrasound time is 60-100 s, and water quenching is conducted immediately after the ultrasound treatment is completed. Grains of semi-solid structures obtained through the method are finer, rounder, more complete and more uniform in distribution and fully meet the requirements for semi-solid rheoforming, operation is easy and convenient, safety and reliability are achieved, and three-waste pollution is avoided.

Description

technical field [0001] The invention belongs to the technical field of metal material preparation and relates to a preparation method of semi-solid slurry. Background technique [0002] Semi-solid forming technology is a near-net forming technology with high production efficiency, and is known as a new generation of metal forming technology in the 21st century. Compared with traditional liquid casting, semi-solid casting has less machining, lower processing temperature, less solidification shrinkage, and significantly improved structure and performance. Studies have shown that adding a small amount of modifiers (such as Na, K, Ba, Sr, Re, etc.) to aluminum alloys can not only achieve better refinement and modification effects, but also have the effect of purifying the melt and degassing, among which Sr is an ideal metamorphic material, its refinement effect is obvious and the metamorphic effect has a long-term effect, that is, the effect of inducing inoculation is very good...

Claims

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Application Information

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IPC IPC(8): B22D1/00
Inventor 闫洪熊俊杰
Owner 江西剑发铝型材有限公司
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