Novel silk swelling agent, and preparation method thereof

A silk bulking agent and a new type of technology, applied in textiles and papermaking, fiber processing, animal fibers, etc., can solve problems such as poor silk softness, fluffy, elasticity, etc., which cannot meet the actual production of factories, etc. Excellent bactericidal performance and outstanding biodegradability

Inactive Publication Date: 2016-03-16
张莘蔓
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is to provide a new type of silk bulking agent and its preparation method, so as to solve the problems that the silk is soft, fluffy, elastic, etc., and cannot meet the actual production needs of the factory after using the silk bulking agent at present.

Method used

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  • Novel silk swelling agent, and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A new type of silk swelling agent, in parts by weight, includes the following raw materials: 525 parts of unwinding agent and 48.3 parts of softening agent. The unwinding agent includes the following raw materials: Na 2 SiO 3 25 parts, 500 parts deionized water; the softener includes the following raw materials: 6 parts of ester quaternary ammonium salt, 0.3 parts of silane-modified polyurethane, 0.2 parts of polyether-modified silane, 0.1 parts of sodium lignosulfonate, alkyl 0.1 part of sodium benzene sulfonate, 0.2 part of sodium starch graft acrylate, 0.2 part of sodium polyacrylate, 0.2 part of sodium N-lauroyl glutamate, 0.2 part of calcium lignosulfonate, 0.2 part of citronellal, 0.3 part of malic acid , 0.1 part of carrageenan, 0.1 part of locust bean gum, 0.1 part of triadimefon, and 40 parts of deionized water.

[0028] The preparation method of the novel silk puffing agent includes the following steps:

[0029] S1: Add the ester quaternary ammonium salt to 40 part...

Embodiment 2

[0036] A new type of silk swelling agent, in parts by weight, includes the following raw materials: 1,050 parts of unwinding agent and 84.8 parts of softening agent. The unwinding agent includes the following raw materials: Na 2 SiO 3 35 parts, 1015 parts of deionized water; the softener includes the following raw materials: 10 parts of ester quaternary ammonium salt, 0.5 parts of silane-modified polyurethane, 0.4 parts of polyether-modified silane, 0.4 parts of sodium lignosulfonate, alkyl 0.3 parts of sodium benzenesulfonate, 0.4 parts of sodium starch graft acrylate, 0.3 parts of sodium polyacrylate, 0.4 parts of sodium N-lauroyl glutamate, 0.3 parts of calcium lignosulfonate, 0.5 parts of citronellal, 0.5 parts of malic acid , 0.3 parts of carrageenan, 0.2 parts of locust bean gum, 0.3 parts of triadimefon, and 70 parts of deionized water.

[0037] The preparation method of the novel silk puffing agent includes the following steps:

[0038] S1: Add the ester quaternary ammonium...

Embodiment 3

[0045] A new type of silk swelling agent, in parts by weight, includes the following raw materials: 780 parts of unwinding agent and 66.6 parts of softening agent. The unwinding agent includes the following raw materials: Na 2 SiO 3 30 parts, 750 parts deionized water; the softener includes the following raw materials: 8 parts ester quaternary ammonium salt, 0.4 parts silane-modified polyurethane, 0.3 parts polyether-modified silane, 0.3 parts sodium lignosulfonate, alkyl 0.2 part of sodium benzene sulfonate, 0.3 part of sodium starch graft acrylate, 0.2 part of sodium polyacrylate, 0.3 part of sodium N-lauroyl glutamate, 0.3 part of calcium lignosulfonate, 0.3 part of citronellal, 0.4 part of malic acid , 0.2 parts of carrageenan, 0.2 parts of locust bean gum, 0.2 parts of triadimefon, and 55 parts of deionized water.

[0046] The preparation method of the novel silk puffing agent includes the following steps:

[0047] S1: Add the ester quaternary ammonium salt to 55 parts of deio...

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Abstract

The invention discloses a novel silk swelling agent, and a preparation method thereof, and belongs to the technical field of swelling agent processing. The novel silk swelling agent comprises, by weight, an unwinding agent and a softener; the unwinding agent comprises Na2SiO3 and deionized water; the softener comprises an ester-based quaternary ammonium salt, silicane-modified polyurethane, polyether modified silicane, sodium lignin sulfonate, sodium alkyl benzene sulfonate, starch grafted sodium acrylate, sodium polyacrylate, sodium N-lauroylglutamate, calcium lignosulphonate, citronellal, malic acid, carrageenan, locust bean gum, triadimefon, and deionized water; and the novel silk swelling agent is prepared via following steps: dissolving of the ester-based quaternary ammonium salt, microwave reaction, defoaming, pH value adjusting, preparing of the unwinding agent, and mixing. After application of the novel silk swelling agent, silk possesses excellent softness and colour intensity; the preparation method is simple; and preparation cost is low.

Description

Technical field [0001] The invention belongs to the technical field of puffing agent processing, and specifically relates to a novel silk puffing agent and a preparation method thereof. Background technique [0002] The traditional method of processing silk quilt is simple, and the variety is extremely single. After the silk quilt processed by traditional technology is used, the silk fibers are easy to entangle and adhere, and the elasticity and warmth retention will be reduced, requiring frequent tearing and tearing. Only by loosening can the original fine clothing performance of the silk quilt be maintained. [0003] In order to endow the silk with excellent bulkiness, softness, high elasticity and other properties, the silk needs to be refined to make the silk fiber voids swelled. The made silk cotton has the characteristics of bulkiness, high elasticity, and no boarding between the fibers. By using a bulking agent to expand the silk, the bulkiness, high elasticity, and flexibi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/79D06M15/564D06M15/647D06M15/01D06M13/256D06M15/11D06M15/263D06M13/13D06M13/192D06M15/03D06M13/352D06M101/12
CPCD06M11/79D06M13/13D06M13/192D06M13/256D06M13/352D06M15/01D06M15/03D06M15/11D06M15/263D06M15/564D06M15/647D06M2101/12
Inventor 张莘蔓
Owner 张莘蔓
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