High-efficiency Fe-SCR integrated catalyst preparation method
A monolithic catalyst and high-efficiency technology, applied in molecular sieve catalysts, chemical instruments and methods, physical/chemical process catalysts, etc., can solve problems such as coatings, and achieve the effect of simple preparation method, improved catalytic performance, and easy steps
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[0029] Example 1: A method for preparing a high-efficiency Fe-SCR monolithic catalyst includes the following steps:
[0030] (1) Fe molecular sieve ion exchange technology
[0031] a. Add FeCl 3 Add to deionized water and mix, heat the water bath to 50℃, wait for FeCl 3 Completely dissolve to obtain the exchange liquid. According to the Fe source / β molecular sieve mass ratio of 0.5, add β molecular sieve to the exchange liquid, continue to heat up to 90°C, and stir evenly for 5 hours for ion exchange;
[0032] b. After the ion exchange is completed, the exchange liquid is cooled and passed into the filter press for washing. After the eluate is colorless, the molecular sieve is placed in an oven and dried at 120°C for 5 hours for use.
[0033] c. Put the dried molecular sieve into a roasting furnace, heat it up to 450 ℃ at a rate of 2 ℃ / min, keep it for 1 hour, and cool it with the furnace for later use to obtain Fe molecular sieve.
[0034] (2) Fully stir the pseudo-boehmite in deionize...
Example Embodiment
[0050] Embodiment 2: A method for preparing a high-efficiency Fe-SCR monolithic catalyst includes the following steps:
[0051] (1) Molecular sieve ion exchange:
[0052] a. Add FeCl 3 Add to deionized water, stir evenly, heat the water bath to 50°C, wait until the Fe source is completely dissolved to make an exchange liquid, according to the Fe source / β molecular sieve mass ratio of 0.6, add β molecular sieve to the exchange liquid, continue heating to 80°C , Stir for 5h for ion exchange;
[0053] b. After the ion exchange is completed, cool the exchange liquid and pass it into the filter press for washing. After the eluate is colorless, put the molecular sieve in an oven and dry at 120°C for 5 hours for later use;
[0054] c. Put the dried molecular sieve into a roaster for roasting, and cool to room temperature after roasting to obtain Fe molecular sieve;
[0055] (2) Add the pseudo-boehmite into the deionized water and stir thoroughly, according to H + / Pseudo-boehmite molar ratio ...
Example Embodiment
[0060] Embodiment 3: A method for preparing a high-efficiency Fe-SCR monolithic catalyst includes the following steps:
[0061] (1) Molecular sieve ion exchange:
[0062] a. The Fe(NO 3 ) 3 Add to deionized water, stir evenly, heat the water bath to 50℃, wait for Fe(NO 3 ) 3 Completely dissolve to make an exchange liquid. According to the Fe source / SSZ-13 molecular sieve mass ratio of 0.7, add molecular sieve to the exchange liquid, continue to heat to 90°C, and stir for 5 hours for ion exchange;
[0063] b. After the ion exchange is completed, cool the exchange liquid and pass it into the filter press for washing. After the eluate is colorless, put the molecular sieve in an oven at 120°C for 6h to be used;
[0064] c. Put the dried molecular sieve into a roaster for roasting, and cool to room temperature after roasting to obtain Fe molecular sieve;
[0065] (2) Add the pseudo-boehmite into the deionized water and stir thoroughly, according to H + / Pseudo-boehmite molar ratio is 0.6, sl...
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