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Method for preparing composite plastic modifying agent based on modified magnesite

A composite plastic and magnesite technology, applied in the field of plastic modifier preparation, can solve the problems of low impact strength, poor elasticity and stress cracking resistance, and achieve good elasticity and stress cracking resistance, good dispersibility, and good preparation. simple method effect

Inactive Publication Date: 2016-04-13
高大元
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Technical problem to be solved by the present invention: Aiming at the disadvantages of low impact strength, poor elasticity and stress cracking resistance of polyethylene and polypropylene general-purpose plastics currently used, a method is provided by pretreating magnesite at high temperature, Then the pretreated magnesite particles are mixed with modifiers, modified under the action of ultrasound, and then modified particles are extracted by filtration, and then natural components are extracted and mixed with modified particles to obtain Method for Compounding Plastic Modifiers

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0016] First, take 600g of magnesite and put it into a pulverizer for crushing, pass through a standard sieve to obtain magnesite particles of 80 mesh, put the obtained particles into a calciner, calcinate for 20min at a temperature of 500°C, and then use a temperature of 5 The hydrogen gas at ℃ lowers the temperature of the calcined particles, and after cooling to room temperature, it is taken out to obtain pretreated magnesite particles; : 1, put into the mixer, with rotating speed 300r / min, high-speed mixing 2min, then the mixture is put into the beaker, then add 50mL dimethyldimethoxysilane and 100mL deionized water therein respectively, stir evenly, Move the container to an ultrasonic oscillator and perform ultrasonic treatment for 30 minutes; after the above ultrasonic treatment is completed, move the container to a water bath, set the temperature at 70°C, and stir it with a stirrer at a set speed of 400r / min , fill it with oxygen, the oxygen filling rate is 8mL / min, sti...

example 2

[0019]First, take 750g of magnesite and put it into a pulverizer for crushing, pass through a standard sieve to obtain magnesite particles of 85 mesh, put the obtained particles into a calciner, calcinate at a temperature of 550°C for 25min, and then use a temperature of 8 The hydrogen gas at ℃ lowers the temperature of the calcined particles, and after cooling to room temperature, it is taken out to obtain pretreated magnesite particles; : 1, put into mixer, with rotating speed 350r / min, high-speed mixing 3min, then mixture is put into beaker, then add 75mL dimethyldimethoxysilane and 110mL deionized water to it respectively, stir evenly, Move the container to an ultrasonic oscillator and perform ultrasonic treatment for 33 minutes; after the above ultrasonic treatment is completed, move the container to a water bath, set the temperature at 80°C, and stir it with a stirrer at a set speed of 500r / min , fill it with oxygen, the oxygen filling rate is 8mL / min, stir and heat for ...

example 3

[0022] First, take 900g of magnesite and put it into a pulverizer for crushing, pass through a standard sieve to obtain 90-mesh magnesite particles, put the obtained particles into a calciner, calcinate for 30min at a temperature of 600°C, and then use a temperature of 10 The hydrogen gas at ℃ lowers the temperature of the calcined particles, and after cooling to room temperature, it is taken out to obtain pretreated magnesite particles; : 1, put into mixer, with rotating speed 400r / min, high-speed mixing 4min, then mixture is put into beaker, then add 80mL dimethyldimethoxysilane and 120mL deionized water therein respectively, stir evenly, Move the container to an ultrasonic oscillator and perform ultrasonic treatment for 35 minutes; after the above ultrasonic treatment is completed, move the container to a water bath, set the temperature at 90°C, and stir it with a stirrer at a set speed of 600r / min , fill it with oxygen, the oxygen filling rate is 8mL / min, stir and heat for...

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PUM

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Abstract

The invention discloses a method for preparing a composite plastic modifying agent based on modified magnesite and belongs to the field of plastic modifying agent preparation. According to the method, pretreatment is performed on the magnesite at high temperature, pretreated magnesite grains are mixed with the modifying agent to achieve modification under the ultrasonication, modified grains are obtained through filtration and extraction, and natural ingredients are extracted to be mixed with the modified grains to obtain the composite plastic modifying agent. The method has the advantages that the preparation method is simple, the obtained composite plastic modifying agent is good in dispersibility, the anti-shock strength of the obtained polyethylene or polypropylene plastic is 8% higher than that of other methods after the composite plastic modifying agent is added into the polyethylene or polypropylene plastic to be used, the elasticity and the stress crack resistance are good, and the method is worth popularizing and utilizing.

Description

technical field [0001] The invention relates to a method for preparing a composite plastic modifier based on modified magnesite, and belongs to the field of plastic modifier preparation. Background technique [0002] Plastic is a high molecular compound polymerized by addition polymerization or polycondensation reaction with monomer as raw material. It is commonly known as plastic or resin. It can freely change its composition and shape. , Colorants and other additives. Polyethylene is a polymer formed by the polymerization of ethylene. The product has been developed for about 60 years. The global polyethylene production ranks first among the five general-purpose resins. It is the most commonly used plastic polymer in the world, with an annual consumption rate of more than 50 billion pounds per year, and more than 70% of Porex products use polyethylene. Polypropylene is a general-purpose plastic used second only to polyethylene. This is mainly because polypropylene has go...

Claims

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Application Information

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IPC IPC(8): C08K9/00C08K9/04C08K9/06C08K9/02C08K3/26C08L23/06C08L23/12
CPCC08K9/00C08K3/26C08K9/02C08K9/04C08K9/06C08K2003/262C08L23/06C08L23/12
Inventor 高大元盛艳花宋国
Owner 高大元
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