Method for preparing composite plastic modifying agent based on modified magnesite
A composite plastic and magnesite technology, applied in the field of plastic modifier preparation, can solve the problems of low impact strength, poor elasticity and stress cracking resistance, and achieve good elasticity and stress cracking resistance, good dispersibility, and good preparation. simple method effect
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example 1
[0016] First, take 600g of magnesite and put it into a pulverizer for crushing, pass through a standard sieve to obtain magnesite particles of 80 mesh, put the obtained particles into a calciner, calcinate for 20min at a temperature of 500°C, and then use a temperature of 5 The hydrogen gas at ℃ lowers the temperature of the calcined particles, and after cooling to room temperature, it is taken out to obtain pretreated magnesite particles; : 1, put into the mixer, with rotating speed 300r / min, high-speed mixing 2min, then the mixture is put into the beaker, then add 50mL dimethyldimethoxysilane and 100mL deionized water therein respectively, stir evenly, Move the container to an ultrasonic oscillator and perform ultrasonic treatment for 30 minutes; after the above ultrasonic treatment is completed, move the container to a water bath, set the temperature at 70°C, and stir it with a stirrer at a set speed of 400r / min , fill it with oxygen, the oxygen filling rate is 8mL / min, sti...
example 2
[0019]First, take 750g of magnesite and put it into a pulverizer for crushing, pass through a standard sieve to obtain magnesite particles of 85 mesh, put the obtained particles into a calciner, calcinate at a temperature of 550°C for 25min, and then use a temperature of 8 The hydrogen gas at ℃ lowers the temperature of the calcined particles, and after cooling to room temperature, it is taken out to obtain pretreated magnesite particles; : 1, put into mixer, with rotating speed 350r / min, high-speed mixing 3min, then mixture is put into beaker, then add 75mL dimethyldimethoxysilane and 110mL deionized water to it respectively, stir evenly, Move the container to an ultrasonic oscillator and perform ultrasonic treatment for 33 minutes; after the above ultrasonic treatment is completed, move the container to a water bath, set the temperature at 80°C, and stir it with a stirrer at a set speed of 500r / min , fill it with oxygen, the oxygen filling rate is 8mL / min, stir and heat for ...
example 3
[0022] First, take 900g of magnesite and put it into a pulverizer for crushing, pass through a standard sieve to obtain 90-mesh magnesite particles, put the obtained particles into a calciner, calcinate for 30min at a temperature of 600°C, and then use a temperature of 10 The hydrogen gas at ℃ lowers the temperature of the calcined particles, and after cooling to room temperature, it is taken out to obtain pretreated magnesite particles; : 1, put into mixer, with rotating speed 400r / min, high-speed mixing 4min, then mixture is put into beaker, then add 80mL dimethyldimethoxysilane and 120mL deionized water therein respectively, stir evenly, Move the container to an ultrasonic oscillator and perform ultrasonic treatment for 35 minutes; after the above ultrasonic treatment is completed, move the container to a water bath, set the temperature at 90°C, and stir it with a stirrer at a set speed of 600r / min , fill it with oxygen, the oxygen filling rate is 8mL / min, stir and heat for...
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