Sponge municipal high-strength high-toughness regenerated aggregate concrete and preparation method thereof
A technology of recycled aggregate and sponge city, applied in the field of building materials, can solve the problems of application limitation, unsatisfactory toughness and crack resistance, low strength, etc., achieve low cost, improve microscopic stress-strain performance, specific surface energy high effect
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Embodiment 1
[0038] First prepare modified silica nanotubes:
[0039] (1) Put 30 stainless steel balls with a diameter of 10mm and 45 stainless steel balls with a diameter of 5mm in two identical 5L nylon tanks, then add 0.9kg of silica nanotubes, and then add 90ml of Water and ethanol, and sealed with a nylon cover; put two ball mill jars symmetrically into the ball mill, and ball mill for 48 hours at a speed of 400rpm and automatically change the direction of rotation every 30 minutes;
[0040] (2) Add the silica nanotubes treated in step (1) into an aqueous solution of Tween 20 with a pH of 8 and a concentration of 20wt% and sonicate for 18 hours, filter, wash with water, and vacuum-dry at 55°C for 15 hours ;
[0041] (3) Take the silicon dioxide nanotubes treated in step (2) and stir in 40L of 35wt% aqueous sodium hydroxide solution for 48 hours, filter, wash the powder with pure water, and dry it in vacuum at 60°C 18h;
[0042] (4) Take the silicon dioxide nanotubes treated in step...
Embodiment 2
[0055] First prepare modified silica nanotubes:
[0056] (1) Put 30 stainless steel balls with a diameter of 10mm and 45 stainless steel balls with a diameter of 5mm in two identical 5L nylon tanks, then add 0.9kg of silica nanotubes, and then add 90ml of Water and ethanol, and sealed with a nylon cover; put two ball mill jars symmetrically into the ball mill, and ball mill for 48 hours at a speed of 400rpm and automatically change the direction of rotation every 30 minutes;
[0057] (2) Add the silica nanotubes treated in step (1) into an aqueous solution of Tween 20 with a pH of 8 and a concentration of 20wt% and sonicate for 18 hours, filter, wash with water, and vacuum dry at 57°C for 15 hours ;
[0058] (3) Take the silica nanotubes treated in step (2) and stir in 40 L of 35 wt% sodium hydroxide aqueous solution for 48 hours, filter, wash the powder with pure water, and dry it in vacuum at 59°C 18h;
[0059] (4) Take the silicon dioxide nanotubes treated in step (3) an...
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