A method for directly mixing pet melts to produce black silk and its special equipment

A technology of melt and black silk, which is applied in melt spinning, rayon manufacturing, textiles and paper making, etc. It can solve the problems of insignificant viscosity reduction, melt viscosity reduction, waste of resources, etc., and achieve good quality stability and quality Stabilize and reduce the effect of coking

Active Publication Date: 2018-04-10
新凤鸣集团股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Aiming at the problems that the current process is easy to cause melt viscosity reduction, complicated process, waste of resources and high cost, the present invention proposes a process such as insignificant viscosity reduction, reduction of slicing and granulation, drying, solid-phase polycondensation, and powder grinding, which greatly Method and special equipment for directly mixing PET melt to produce black silk with reduced electricity, packaging and transportation costs

Method used

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  • A method for directly mixing pet melts to produce black silk and its special equipment
  • A method for directly mixing pet melts to produce black silk and its special equipment

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Embodiment 1 A kind of PET melt of the present invention directly mixes and prepares the method for black silk, comprises the steps:

[0030] Step 1. Introduce a melt with a viscosity of 0.63dl / g from the PET main melt pipeline, and mix in matting agent (49%) and dispersant (1%) according to the mass ratio to obtain a compound; mix in matting agent and dispersant in proportion , to obtain the mixture, the mass ratio of the melt: matting agent: dispersant is 1:0.49:0.01; the melt is PET, the matting agent is titanium dioxide, and the dispersant is titanic acid Ester coupling agent;

[0031] Step 2. The mixture obtained in step 1 is entered into a twin-screw extruder under negative pressure for low-speed (120rpm) initial mixing to form an initial mixing melt;

[0032] Step 3. The primary mixed melt coming out of the screw extruder is first blended by an ultrasonic dynamic mixer to obtain a mixed melt;

[0033] Step 4. The mixed melt is then input into the PET main melt ...

Embodiment 2

[0036] Example 2 The special equipment constructed by the method described in Example 1, including extruder assembly 1, auxiliary material bin assembly 2, dispersant bin assembly 3, ultrasonic dynamic mixing assembly 4, dynamic mixing assembly 5 , the spinning metering assembly 6 and the control box, the main melt pipeline 7 is connected to the discharge port of the discharge assembly 8, and the main melt pipeline 7 is connected with the extruder assembly through the branch melt pipeline 71 The first feeding port of 1 is communicated with the pipeline, the feeding port of the auxiliary material bin assembly 2 is configured with the first feeding assembly 91, and the feeding port of the dispersant bin assembly 3 is configured with the second feeding port. material assembly 92, and the discharge opening of the first feeding assembly 91 and the second feeding assembly 92 are all in communication with the second feed inlet pipeline of the extruder assembly 1, the extruder assembly ...

Embodiment 3

[0053] Example 3 Contrast of conventional masterbatch preparation and melt preparation masterbatch

[0054] 1. Cases of conventional masterbatch addition:

[0055] Black silk, output 48 tons / day:

[0056] Buy masterbatch (masterbatch concentration 30%), masterbatch viscosity 0.4dl / g, send into single-screw extruder after drying and melting, the screw extruder rotating speed controls outlet pressure. After metering, the masterbatch melt enters the main melt pipeline with an addition amount of 3% of the fiber, and is spun after being efficiently blended by a dynamic mixer, and the dynamic mixer speed is set at 35 rpm. The maintenance period is 3 months. The cost of black silk increases by 360 yuan / ton on the basis of white silk.

[0057] 2. Cases of direct addition of powder to prepare functional fibers:

[0058] Black silk, output 48 tons / day:

[0059] The melt with a viscosity of 0.62dl / g is introduced from the main melt pipeline, and the introduced melt is first metered by...

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Abstract

Provided are a method for preparing black yarn through direct mixing of a PET melt and special equipment of the method. The method comprises the steps that a melt is introduced from a main melt pipeline, and then a delustering agent and a dispersing agent are mixed according to a proportion; the mixture enters a double screw extruder under a negative pressure condition to be subjected to low-speed primary mixing, co-blending is conducted through an ultrasonic dynamic mixing machine, and direct spinning is conducted after mixing is conducted through a dynamic mixer. The equipment comprises an extruder assembly, an auxiliary material bin assembly, a dispersing agent bin assembly, an ultrasonic dynamic mixing assembly, a dynamic mixing assembly, a spinning metering assembly and a control box; the main melt pipeline is connected to a material outlet of a material outlet assembly, a material outlet of the ultrasonic dynamic mixing assembly is connected with the main melt pipeline through a tee joint and then communicated with the dynamic mixer, a material outlet of the dynamic mixer is communicated with a material inlet of a spinning metering pump, and a material outlet of the spinning metering pump serves as a spinning assembly connector to be connected with spinning equipment. The method for preparing the black yarn through direct mixing of the PET melt and the special equipment of the method have the advantages that the viscosity is reduced, the quality is stable, the spinnability is good, and the cost is low.

Description

technical field [0001] The invention relates to a method for directly mixing PET melts to prepare black silk and special equipment thereof. Background technique [0002] In the past, functional fibers were produced through the chip spinning process, using white chips and functional masterbatches for melt spinning. In recent years, with the maturity of melt direct spinning pipeline addition technology, the dual advantages of quality and cost of melt direct spinning are gradually replacing chip spinning as the main production route of functional fibers. However, the twin-screw extrusion process involved in the traditional process requires high-speed rotation and mixing, which makes the viscosity of the melted raw materials drop significantly under the shearing effect of high-speed rotation, so it is necessary to choose high-viscosity slice compensation in the selection of raw materials. The loss of viscosity reduction during the tablet making process leads to high spinning co...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01D5/08D01F1/10
CPCD01D5/08D01F1/10D01F1/106
Inventor 庄耀中赵春财孙建杰韩梅
Owner 新凤鸣集团股份有限公司
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