Magnesium indium phosphate matrix material for rare earth phosphor and preparation method thereof
A technology of magnesium indium phosphate and rare earth phosphors, which is applied in the direction of luminescent materials, chemical instruments and methods, etc., can solve the problems of rare exploration of new matrix materials, and achieve the effect of simple preparation process
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Embodiment 1
[0039] Example 1: Mg 25 In 30 P 45 o 182.5 Preparation of Phosphor Matrix
[0040] Weigh 0.1947g MgO, 0.8049g In 2 o 3 , 1.0004g NH 4 h 2 PO 4 Put it in a beaker, add an appropriate amount of nitric acid to dissolve the raw materials, add a small amount of polyvinyl alcohol and an appropriate amount of deionized water after the solution is clarified, heat and stir until it is completely evaporated to dryness, dry the beaker in a drying oven and grind it evenly; then carry out two final steps Sintering (the sintering temperature of the first stage is 1200°C, after 15 hours of heat preservation, it is cooled to room temperature with the furnace, and ground for 10 minutes; the sintering temperature of the second stage is 1200°C, and it is cooled to room temperature with the furnace after 15 hours of heat preservation, and the heating rate of the two steps of sintering is 5 °C / min). Take out the burnt sample and grind it to get Mg 25 In 30 P 45 o 182.5 Phosphor matrix...
Embodiment 2
[0041] Example 2: Mg 23 In 29 P 44 o 176.5 Preparation of Phosphor Matrix
[0042] Weigh 0.1851g MgO, 0.8040g In 2 o 3 , 1.0108g NH 4 h 2 PO 4 , the rest of the steps are the same as in Example 1.
Embodiment 3
[0043] Example 3: Mg 27 In 33 P 47 o 194 Preparation of Phosphor Matrix
[0044] Weigh 0.1965g MgO, 0.8272g In 2 o 3 , 0.9763g NH 4 h 2 PO 4 , the rest of the steps are the same as in Example 1.
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