Graphene strengthening nickel base composite material and preparing method thereof

A composite material and graphene technology, which is applied in the field of graphene-enhanced nickel-based composite materials and its preparation, can solve problems such as graphene-enhanced nickel-based composite materials that have not yet been seen, achieve breakthroughs in scientific and technical problems, and avoid agglomeration and damage , evenly distributed effect

Active Publication Date: 2016-06-22
SHANGHAI HIWAVE COMPOSITE MATERIALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] So far, there is no technology to prepare graphene

Method used

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  • Graphene strengthening nickel base composite material and preparing method thereof

Examples

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Comparison scheme
Effect test

Embodiment 1

[0041] The basic operation steps of present embodiment 1 preparation graphene reinforced nickel-based composite material are as follows:

[0042] Ⅰ) Material composition of graphene-reinforced nickel-based composites

[0043] The material components of graphene-enhanced nickel-based composites are mainly metallic nickel and graphene, in which metallic nickel is prepared by chemical reduction method, with a particle size of 0.1μm-5μm, accounting for 94wt% of the composite material; the raw material of graphene is The single-layer or few-layer graphene oxide prepared by the Hummers method accounts for 6wt% in the composite material. Of course, graphene oxide prepared by other methods may also be used in other embodiments, and is not limited to the Hummers method.

[0044] Ⅱ) Basic steps for preparing graphene-reinforced nickel-based composites (see attached figure 1 )

[0045] 1) Prepare 0.1mol / L nickel sulfate solution and 0.1mol / L ascorbic acid solution (or one or more of g...

Embodiment 2

[0052] The main difference from Example 1 is that this Example 2 adds a hot extrusion process to obtain a graphene / nickel composite wire.

[0053] The basic operation steps of present embodiment 2 preparing graphene / nickel composite wire material are as follows:

[0054] Ⅰ) Material composition of graphene-reinforced nickel-based composites

[0055] The material components of graphene-enhanced nickel-based composites are mainly metallic nickel and graphene, in which metallic nickel is prepared by chemical reduction method, with a particle size of 0.1 μm-5 μm, accounting for 97wt% of the composite material; the raw material of graphene is The single-layer or few-layer graphene oxide prepared by the Hummers method accounts for 3wt% in the composite material.

[0056] Ⅱ) Basic steps for preparing graphene-reinforced nickel-based composites (see attached figure 1 )

[0057] 1) Prepare 0.25mol / L nickel sulfate solution and 0.25mol / L ascorbic acid solution;

[0058] 2) adding gr...

Embodiment 3

[0065] The difference from Example 2 is that this Example 3 adds an annealing and rolling process on the basis of Example 2 to obtain a graphene / nickel composite strip.

[0066] The basic operation steps of present embodiment 3 preparation graphene / nickel composite strips are as follows:

[0067] Ⅰ) Material composition of graphene-reinforced nickel-based composites

[0068] The material components of the graphene-enhanced nickel-based composite material are mainly metallic nickel and graphene, wherein the raw materials and contents of metallic nickel and graphene are the same as those in Example 2.

[0069] Ⅱ) Basic steps for preparing graphene-reinforced nickel-based composites (see attached figure 1 )

[0070] 1) Prepare 0.25mol / L nickel sulfate solution and 0.25mol / L ascorbic acid solution;

[0071] 2) adding graphene oxide into deionized water, stirring and dispersing the ions for 0.5 hours to uniformly disperse the graphene oxide to obtain a graphene oxide solution wi...

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Abstract

The invention discloses a graphene strengthening nickel base composite material and a preparing method thereof. The method includes the steps that a reducing agent and nickel sulfate are sequentially added into an oxidized graphene solution; nickel powder prepared through reduction is directly compounded with oxidized graphene in the solution, and oxidized graphene/nickel composite powder is initially obtained; the oxidized graphene/nickel composite powder is dried and restored to obtain graphene/nickel composite powder; and composite blocks, composite wires and composite strips of graphene/nickel are obtained through powder metallurgy, hot extrusion and rolling technologies. Graphene in the composite material is evenly scattered, base and strengthening body interface bonding is good, and the composite material has the excellent physical performance. Meanwhile, the process of the graphene strengthening nickel base composite material and the preparing method is simple, the procedure is easy to control, and large-scale application and production are easy to achieve.

Description

technical field [0001] The invention relates to a method for preparing a metal-based composite material in the field of material technology, in particular to a graphene-reinforced nickel-based composite material and a preparation method thereof. Background technique [0002] In the field of aerospace, high-temperature alloy materials represented by nickel alloys are widely used in the main load-carrying components of aircraft, aero-engines, aviation fire control systems, hot-end components of advanced propulsion systems, and high-temperature key components of other equipment. With the development of the aerospace industry, especially with the development of national defense weapons and equipment in the direction of high performance and high efficiency, actual engineering has higher and higher requirements for the comprehensive performance of high-temperature materials, making it difficult for a single material to meet actual needs. Due to the advantages of good high temperat...

Claims

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Application Information

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IPC IPC(8): C22C1/05C22C19/03B22F9/24B22F3/10C22C1/10B22F3/24
CPCB22F3/10B22F3/24B22F9/24B22F2998/10B22F2999/00C22C1/05C22C19/03B22F3/1007B22F2201/013B22F3/02
Inventor 王鹏鹏毛琳陈乐生沈敏华
Owner SHANGHAI HIWAVE COMPOSITE MATERIALS CO LTD
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