A three-dimensional interpenetrating al by in situ reaction 2 o 3 /al composite approach
A composite material and in-situ reaction technology, applied in the field of materials, can solve the problems of uneven dispersion, different performance, uneven distribution of reinforcement particles, etc., and achieve the effect of improving wear resistance, clear interface and good combination
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Embodiment 1
[0029] (1) SiO 2 Preparation of ceramic slurry: Weigh 70g of analytically pure 200 mesh SiO 2 Powder, weigh 7g H 3 BO 3 , weigh 0.3g carboxymethyl cellulose, measure 30mL water, measure 4.9mL ammonium polyacrylate, mix the weighed materials and stir evenly, pour them into the mixing bottle, add ceramic balls and wet grind on the mixer 24h, get SiO 2 Ceramic slurry;
[0030] (2) The pretreatment of polyurethane foam: get hole number and be that 10ppi polyurethane foam soaks 5h in the NaOH solution of 20% in mass fraction, knead the thin film between polyurethane foam ribs, then immerse in the PVA solution of 5% in mass fraction Activation treatment at 60°C for 24h.
[0031] (3) Slurry: immerse the pretreated polyurethane foam in SiO 2 Carry out vacuum impregnation and slurrying in the ceramic slurry, the vacuum degree is -0.1MPa, and the dipping time is 5 minutes. After slurrying, the green body is taken out and dried at room temperature and normal pressure to obtain a dr...
Embodiment 2
[0035](1) SiO 2 Preparation of ceramic slurry: Weigh 70g of analytically pure 200 mesh SiO 2 Powder, weigh 7g H 3 BO 3 , weigh 0.3g carboxymethyl cellulose, measure 30mL water, measure 4.9mL ammonium polyacrylate, mix the weighed materials and stir evenly, pour them into the mixing bottle, add ceramic balls and wet grind on the mixer 24h, get SiO 2 Ceramic slurry;
[0036] (2) The pretreatment of polyurethane foam: get hole number and be that 20ppi polyurethane foam soaks 5h in the NaOH solution of 20% in mass fraction, knead the thin film between the tendons of polyurethane foam, then immerse in the PVA solution of 5% in mass fraction Activation treatment at 60°C for 24h.
[0037] (3) Slurrying: immerse the pretreated polyurethane foam into the SiO2 ceramic slurry for vacuum impregnation and slurrying. The vacuum degree is -0.1 MPa, and the immersion time is 5 minutes. After slurrying, the green body is taken out, and dried at room temperature and normal pressure to obt...
Embodiment 3
[0041] (1) SiO 2 Preparation of ceramic slurry: Weigh 70g of analytically pure 200 mesh SiO 2 Powder, weigh 7g H 3 BO 3 , weigh 0.3g carboxymethyl cellulose, measure 30mL water, measure 4.9mL ammonium polyacrylate, mix the weighed materials and stir evenly, pour them into the mixing bottle, add ceramic balls and wet grind on the mixer 24h, get SiO 2 Ceramic slurry;
[0042] (2) The pretreatment of polyurethane foam: get hole number and be that 30ppi polyurethane foam soaks 5h in the NaOH solution of 20% in mass fraction, knead the film between polyurethane foam tendons, then immerse in the PVA solution of 5% in mass fraction Activation treatment at 60°C for 24h.
[0043] (3) hanging paste: the pretreated polyurethane foam is immersed in the SiO 2 Carry out vacuum impregnation and slurrying in the ceramic slurry, the vacuum degree is -0.1MPa, and the dipping time is 5 minutes. After slurrying, the green body is taken out, and dried at room temperature and normal pressure ...
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