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Negative waterborne coating emulsion and production process thereof

A water-based coating and production process technology, applied in the direction of anti-corrosion coatings, electrophoretic coatings, epoxy resin coatings, etc., can solve the problem of uneven film thickness distribution of electrophoretic coatings, small particles prone to appear in the dispersion process, and low electrophoretic transmittance of emulsions, etc. problem, to achieve the effect of increasing the anti-corrosion effect, improving the anti-corrosion effect, and good coloring effect

Active Publication Date: 2016-07-20
WEIFANG HELI WATER BASED PAINT MAKING CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] 1. The penetration rate of emulsion electrophoresis is low, the thickness distribution of the electrophoretic coating film is not uniform, and there will be gaps in the paint film on some parts, resulting in poor anti-corrosion effect;
[0004] 2. The texture of the emulsion is rough, the leveling and ductility are poor, which affects the quality of the paint film;
[0005] 3. In the process of emulsion production, it is easy to produce shrinkage cavities, which will lead to a decline in product quality, and will also lead to unevenness of the paint film when the paint is used in the later stage;
[0006] 4. In the process of emulsion production, heating and heat preservation are required so that the reaction between the various raw materials can proceed normally, but during the process of heating and heat preservation, the solvent is easy to volatilize, resulting in waste of production raw materials and environmental pollution. loss and inconvenience to the business;
[0007] 5. In the process of emulsion production, the initial reaction temperature is high, and the temperature required for neutralization by adding carboxylic acid in the later stage is low, resulting in low production efficiency, and small particles are prone to appear during the dispersion process

Method used

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  • Negative waterborne coating emulsion and production process thereof
  • Negative waterborne coating emulsion and production process thereof
  • Negative waterborne coating emulsion and production process thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0051] A negative water-based paint emulsion is made from the following raw materials:

[0052]

[0053]

[0054] The production process includes the following steps:

[0055] Step 1: Add the prescribed amount of epoxy resin, methyl ether and isooctyl alcohol into the epoxy kettle for melting epoxy resin, heat up to 60°C, start stirring, and continue to heat up until the epoxy resin in the kettle is completely melted At this time, the temperature is about 110°C. Open the lid of the epoxy kettle to confirm that the epoxy resin is completely melted.

[0056] Step 2: Put all the melted epoxy resin into the reaction kettle, raise the temperature to 80°C, add the formula amount of diethanolamine, and keep it warm for 2 hours at this temperature.

[0057] Step 3: After the heat preservation is completed, add the formulated amount of polyamine resin, then raise the temperature to 100° C., and heat the reaction for 2 hours.

[0058] Step 4: After the heat preservation reaction...

Embodiment 2

[0062] A negative water-based paint emulsion is made from the following raw materials:

[0063]

[0064] The production process includes the following steps:

[0065] Step 1: Add the prescribed amount of epoxy resin, methyl ether and isooctyl alcohol into the epoxy kettle used to melt the epoxy resin, heat up to 65°C, start stirring, and continue to heat up until the epoxy resin in the kettle is completely melted At this time, the temperature is about 110°C. Open the lid of the epoxy kettle to confirm that the epoxy resin is completely melted.

[0066] Step 2: Put all the melted epoxy resin into the reaction kettle, raise the temperature to 85°C, add the formula amount of diethanolamine, and keep it warm for 2.5 hours at this temperature.

[0067] Step 3: After the heat preservation is completed, add the formulated amount of polyamine resin, then raise the temperature to 101° C., and heat the reaction for 2.2 hours.

[0068] Step 4: After the heat preservation reaction is...

Embodiment 3

[0072] A negative water-based paint emulsion is made from the following raw materials:

[0073]

[0074] The production process includes the following steps:

[0075] Step 1: Add the prescribed amount of epoxy resin, methyl ether and isooctyl alcohol into the epoxy kettle used to melt the epoxy resin, heat up to 70°C, start stirring, and continue to heat up until the epoxy resin in the kettle is completely melted At this time, the temperature is about 110°C. Open the lid of the epoxy kettle to confirm that the epoxy resin is completely melted.

[0076] Step 2: put all the melted epoxy resin into the reaction kettle, raise the temperature to 83°C, add the formula amount of diethanolamine, and keep it warm for 2.2 hours at this temperature.

[0077] Step 3: After the heat preservation is completed, add the formulated amount of polyamine resin, then raise the temperature to 99° C., and heat the reaction for 2.5 hours.

[0078] Step 4: After the heat preservation reaction is ...

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Abstract

The invention discloses negative waterborne coating emulsion and a production process thereof, belonging to the technical field of anticorrosive coatings. The emulsion comprises 13-21 parts of epoxy resin, 5-9 parts of methyl ether, 1-1.5 parts of isooctyl alcohol, 1-1.5 parts of diethanol amine and 3-6 parts of polyamine resin by weight and is prepared by carrying out chemical reaction and mixing on the components, then carrying out neutralization with 1.5-3 parts by weight of carboxylic acid and then carrying out dispersion in 38-60 parts by weight of deionized water. The emulsion and the production process have the beneficial effects that the loss is low in the emulsion production process, thus reducing the production cost; the emulsion has high throwing power and good levelling property and ductility; and the production process is high in production efficiency and has the effect of improving the product quality.

Description

technical field [0001] The invention relates to the technical field of anti-corrosion coatings, in particular to a cathode water-based coating emulsion and a production process thereof. Background technique [0002] In cathodic electrophoretic coatings, resin emulsion is the main film-forming substance, which determines the film performance of cathodic electrophoretic coatings, and has always been the focus of people's research and development. At present, the resin emulsion still has the following deficiencies in practical application: [0003] 1. The penetration rate of emulsion electrophoresis is low, the thickness distribution of the electrophoretic coating film is not uniform, and there will be gaps in the paint film on some parts, resulting in poor anti-corrosion effect; [0004] 2. The texture of the emulsion is rough, the leveling and ductility are poor, which affects the quality of the paint film; [0005] 3. In the process of emulsion production, it is easy to pr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D163/00C09D175/08C09D5/08C09D5/44C09D7/12C09D7/00
CPCC08L2205/035C09D5/08C09D5/4457C09D5/4492C09D7/20C09D7/63C09D7/65C09D163/00C08L75/08C08L79/02C08K5/17C08K5/09
Inventor 张希良谢俊
Owner WEIFANG HELI WATER BASED PAINT MAKING CO LTD
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