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Preparation method of deacidifying agent with lotus leaves

A deacidification agent and lotus leaf technology, which is applied in the field of preparation of lotus leaf deacidification agent, can solve the problems of easy decomposition, large limitation, inability to effectively remove oleic acid, etc., and achieves no environmental pollution and simple preparation process. Effect

Active Publication Date: 2016-08-10
湖北香满宇生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention: Aiming at the problem that the current adsorption deacidification agent has single effect and large limitations, cannot meet the requirements of effective removal of oleic acid, and is easy to decompose during the adsorption process, a new method is provided by decomposing fresh lotus leaves. Drying and grinding, extracting nuciferine under the action of ultrasound, and then activating the dried lotus leaf by grinding to prepare a microporous deacidification agent carrier, by compounding nuciferine and the microporous deacidification agent carrier, the nuciferin Loaded on the activated lotus leaf deacidifier carrier to effectively remove vegetable oleic acid

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0017] First collect fresh lotus leaves, dry them at 85°C for 6 hours, then grind and sieve them to prepare 50-mesh lotus leaf powder, then stir the lotus leaf powder with absolute ethanol at a mass ratio of 1:10 Mix it, heat it in a water bath at 65°C for 10 minutes; after the heating is completed, apply 300W ultrasonic treatment to it for 10 minutes, then add dropwise 0.2mol / L hydrochloric acid solution with 50% lotus leaf powder mass, and control the dropping time for 10 minutes , after the dropwise addition is completed, heat it for 2 hours; after the heat preservation is completed, filter it and collect the filtrate, adjust the pH to 8.5 with a mass concentration of 2% ammonia solution, stir and mix until it completely precipitates, filter it and collect it Filtrate, according to the volume ratio of 1:5, stir and mix the filtrate with absolute ethanol, then filter with a 0.50 μm filter membrane and collect the filtrate, and place it at 75°C for rotary evaporation to drynes...

example 2

[0020] First collect fresh lotus leaves, dry them at 87°C for 7 hours, then grind and sieve them to prepare 55-mesh lotus leaf powder, then stir the lotus leaf powder with absolute ethanol at a mass ratio of 1:10 Mix and heat it in a water bath at 72°C for 12 minutes; after the heating is completed, apply 350W ultrasonic treatment for 12 minutes, then add dropwise 0.2mol / L hydrochloric acid solution with 50% lotus leaf powder mass, and control the dropping time for 12 minutes , after the dropwise addition is completed, heat it for 2 hours; after the heat preservation is completed, filter it and collect the filtrate, adjust the pH to 8.5 with a mass concentration of 2% ammonia solution, stir and mix until it completely precipitates, filter it and collect it Filtrate, according to the volume ratio of 1:5, the filtrate is stirred and mixed with absolute ethanol, then filtered with a 0.50 μm filter membrane and the filtrate is collected, and it is placed at 77 ° C and rotated to dr...

example 3

[0023] First collect fresh lotus leaves, dry them at 90°C for 8 hours, then grind and sieve them to prepare 60-mesh lotus leaf powder, then stir the lotus leaf powder with absolute ethanol at a mass ratio of 1:10 Mix and heat it in a water bath at 80°C for 15 minutes; after the heating is completed, apply 400W ultrasonic treatment for 15 minutes, then add dropwise 0.2mol / L hydrochloric acid solution with 50% lotus leaf powder mass, and control the dropping time for 15 minutes , after the dropwise addition is completed, heat it for 3 hours; after the heat preservation is completed, filter it and collect the filtrate, adjust the pH to 8.5 with a mass concentration of 2% ammonia solution, stir and mix until it completely precipitates, filter it and collect it Filtrate, according to the volume ratio of 1:5, the filtrate and absolute ethanol are stirred and mixed, then filtered with a 0.50 μm filter membrane and the filtrate is collected, and it is placed at 80 ° C and rotated to dr...

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Abstract

The invention relates to a preparation method of a deacidifying agent with lotus leaves and belongs to the technical field of preparation of the deacidifying agent. For solving the problem that an adsorption deacidifying agent in the prior art has single effect and high limitation, cannot effectively remove oleic acid, and is liable to decompose during adsorption. The preparation method includes the steps of: drying and grinding fresh lotus leaves, extracting nuciferine under ultrasonic wave, grinding and activating dried lotus leaves to prepare a microporous deacidifying agent supporter, and compositing the nuciferine with the microporous deacidifying agent supporter to support the nuciferine onto the activated deacidifying agent supporter to effectively remove oleic acid in plants. The deacidifying agent has low oil loss rate being only 0.1% and is improved in adsorption efficiency by 25-30% than other deacidifying agents, is simple in preparation process, is green and environment-friendly and is free of environment pollution.

Description

technical field [0001] The invention relates to a preparation method of lotus leaf deacidification agent, belonging to the technical field of deacidification agent preparation. Background technique [0002] Oil refining is to process a certain quality of oil to be refined into finished oil that meets the quality requirements. The essence of this process is to remove the non-neutral oil components in the oil to be refined, so as to obtain relatively pure finished oil, that is, neutral oil. Purification process. Generally speaking, oil refining mainly includes oil filtration, degumming, deacidification, decolorization, deodorization, winterization, dewaxing and other processes. Among them, the oil that has been filtered, degummed, and deacidified is called semi-refined oil, while the oil that has been decolorized, deodorized, winterized, and dewaxed is called refined oil. Generally, unrefined crude oil contains a certain amount of free fatty acid, and the process of removing...

Claims

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Application Information

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IPC IPC(8): B01J20/24B01J20/30C11B3/10C11B3/00
CPCB01J20/22B01J20/24B01J2220/44B01J2220/4812B01J2220/4825B01J2220/485C11B3/001C11B3/10
Inventor 董晓高力群
Owner 湖北香满宇生物科技有限公司
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