Preparation method of tobacco substrate realizing non combustion after being heated and containing microcapsule
A heat-not-burn, micro-encapsulation technology, applied in the field of tobacco, can solve the problems of reducing the amount of tar and harmful substances released, and increasing the amount of smoke of heat-not-burn tobacco products, so as to improve the aroma concentration and smoke experience, and ensure the quality stability. Effect
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Embodiment 1
[0027] Weigh 100g of flue-cured tobacco powder and place it in a 1L Erlenmeyer flask, add 300mL of 90% ethanol, ultrasonically extract for 4 hours at an ultrasonic frequency of 40KHz and a temperature of 50°C, after standing and settling, first filter through a sand core funnel and then Filter the filtrate with a microporous membrane with a pore size of 0.45 μm, and concentrate it by rotary evaporation under reduced pressure to obtain the initial tobacco extract; the initial extract is refined and extracted by molecular distillation to obtain the final tobacco essential oil. The molecular distillation conditions are as follows: feed rate 5m L / min, vacuum degree 18Pa, sample injection temperature 80°C, heating temperature 80°C, cooling temperature 10°C, rotation speed 350r / min.
[0028] Weigh 50g of gelatin and gum arabic, and make them into aqueous solutions with a weight concentration of 1%. Mix the tobacco essential oil obtained by molecular distillation with triacetin at a...
Embodiment 2
[0032] Weigh 100g of oriental tobacco powder into a 1L Erlenmeyer flask, add 300mL of 90% ethanol, ultrasonically extract at an ultrasonic frequency of 40KHz and a temperature of 50°C for 4 hours, after standing and settling, first filter through a sand core funnel Then filter the filtrate with a microporous filter membrane with a pore size of 0.45 μm, concentrate by rotary steaming under reduced pressure, and obtain the initial tobacco extract; carry out the refined extraction of the initial extract with molecular distillation to obtain the final tobacco essential oil, and the molecular distillation conditions are as follows: feed rate 5m L / min, vacuum degree 18Pa, sample injection temperature 80°C, heating temperature 80°C, cooling temperature 10°C, rotation speed 350r / min.
[0033] Weigh 50g of gelatin and gum arabic, and make them into aqueous solutions with a concentration of 3% by weight respectively. Mix the tobacco essential oil obtained by molecular distillation with ...
Embodiment 3
[0037] Weigh 100g of Burley tobacco powder into a 1L Erlenmeyer flask, add 300mL of 90% ethanol, ultrasonically extract at an ultrasonic frequency of 40KHz and a temperature of 50°C for 4 hours, let it settle, and then filter through a sand core funnel Then filter the filtrate with a microporous filter membrane with a pore size of 0.45 μm, concentrate by rotary steaming under reduced pressure, and obtain the initial tobacco extract; carry out the refined extraction of the initial extract with molecular distillation to obtain the final tobacco essential oil, and the molecular distillation conditions are as follows: feed rate 5m L / min, vacuum degree 18Pa, sample injection temperature 80°C, heating temperature 80°C, cooling temperature 10°C, rotation speed 350r / min.
[0038]Weigh 50g of gelatin and gum arabic, and make them into aqueous solutions with a weight concentration of 0.1%. Mix the tobacco essential oil obtained by molecular distillation with triacetin at a ratio of 1:15...
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