Phase-change heat-storage composite material for hot compress
A composite material and phase change heat storage technology, applied in heat exchange materials, heating appliances for therapeutic treatment, cooling appliances for therapeutic treatment, etc., can solve problems such as burns, save a lot of cost, and the raw materials are convenient and easy to obtain , the effect of not easy to store containers
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[0069] According to the present invention, a preparation method of the above-mentioned phase change heat storage composite material and a phase change heat storage composite material prepared by the method are also provided, and the preparation method includes the following steps:
[0070] 1. Weigh cetyl alcohol, surfactant and water, preferably at 50-60°C, according to the above weight ratio,
[0071] 2. Put the surfactant in a container, and then add an inorganic solvent, preferably water,
[0072] 3. Add cetyl alcohol, preferably under stirring conditions, more preferably added in batches or dropwise, the stirring speed is 300-1000rpm,
[0073] 4. Mix the above components, preferably by continuing stirring or ultrasonic oscillation to uniformly mix the components, more preferably the ultrasonic oscillation frequency is 100-800W, to prepare a microemulsion phase change heat storage composite material.
[0074] According to the present invention, in the process of preparing the phase c...
Example Embodiment
[0103] Example 1
[0104] Weigh 6.00g cetyl alcohol, 1.00g Tween-80, and 1.5g water at 50-60°C,
[0105] Put the weighed Tween-80 in a beaker, add the weighed water to it,
[0106] Add the weighed cetyl alcohol dropwise under stirring conditions, add the weighed cetyl alcohol in 6 times under stirring conditions, add 1 g each time, stirring at intervals of 30 seconds,
[0107] The above components are fully mixed uniformly to prepare a microemulsion phase change heat storage composite material.
[0108] (1) DSC analysis of the prepared phase change heat storage composite material, the procedure is:
[0109] 1) Constant temperature at 80℃; 2) 10℃ / min down to 0℃, the result is as follows figure 2 Shown. by figure 2 It can be clearly seen that the enthalpy value is 177.4J / g, and the freezing point is 44.92°C, 39.15°C.
[0110] (2) The phase change heat storage composite material was characterized by infrared spectroscopy, and the results are as follows image 3 As shown, 3321cm -1 , 2955c...
Example Embodiment
[0111] Example 2
[0112] Weigh 6.00g cetyl alcohol, 1.00g Tween-80, and 2.5g glycerin at 50-60°C,
[0113] Place the weighed Tween-80 in a beaker, add the weighed glycerin to it at once,
[0114] After fully stirring to fully dissolve Tween-80, add the weighed cetyl alcohol in 6 times under stirring conditions, adding 1g each time, stirring at intervals of 30 seconds.
[0115] Continue to stir to make the above-mentioned components fully mixed uniformly, and prepare a microemulsion phase change heat storage composite material.
[0116] (1) DSC analysis of the prepared phase change heat storage composite material, the procedure is:
[0117] 1) Constant temperature at 80℃; 2) 10℃ / min down to 0℃, the result is as follows Figure 4 Shown. by Figure 4 It can be clearly seen that the enthalpy value is 173.6J / g, and the freezing point is: 43.99°C, 40.24°C.
[0118] (2) The phase change heat storage composite material was characterized by infrared spectroscopy, and the results are as follows ...
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