Recycling method of silicon carbide micropowder in filter cake of filter press
A medium silicon carbide, filter press technology, applied in the direction of silicon carbide, carbide, etc., can solve the problems of affecting the plant environment and waste of resources, and achieve the effect of improving the plant environment, increasing the content of silicon carbide, and increasing the content of
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Embodiment 1
[0019] Example 1: A method for recycling silicon carbide micropowder in filter cake of filter press, including the following steps:
[0020] (1) In a 5L pickling tank, add 2000kg of filter cake, and inject 4000kg of 70-80℃ water, stir to make all the added filter cake dissolve and make the slurry evenly distributed.
[0021] (2) Add 400kg of sulfuric acid to the slurry obtained in step (1), stir for 30 minutes, stop the stirring after the sulfuric acid and the slurry are evenly mixed, and after soaking for 5-8 hours, detect the free carbon and free iron in the silicon carbide powder in the slurry When the iron content is less than 0.15% and the carbon content is less than 0.40%, the upper clarified water is discharged.
[0022] (3) Pour 4000 kg of 70-80°C water into the material obtained in step (2), add 160 kg of sodium hydroxide after stirring, and continue stirring. After the alkali and the slurry are fully mixed, stop stirring and soak for 2 to 3 hours. Remove the silicon powder...
Embodiment 2
[0025] Embodiment 2: A method for recycling silicon carbide micropowder in the filter cake of a filter press. The difference from Embodiment 1 is that the acid added in step (2) is nitric acid, phosphoric acid or hydrochloric acid.
Embodiment 3
[0026] Example 3: A method for recycling silicon carbide powder in the filter cake of a filter press, which is different from Example 1 in that the acid added in step (2) is at least two of sulfuric acid, nitric acid, phosphoric acid, and hydrochloric acid mixture.
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